GCMS analysis results for sample AE01505, Mar 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2102\1505.D Vial: 28 Acq On : 22 Feb 2002 6:45 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ***************************** * *************************************** Peak Number 2 Phosphonic acid, dioctadecyl e Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.97 0.60 ug/1 50594 Phenanthrene-dl0 25.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 /95 2 1-Octadecanol 270 C18H380 000112-92-5 95 3 1-Nonadecanol 284 C19H40O 001454-84-8 94' 4 1-Heptadecanol 256 C17H360 001454-85-91 43.05100. 00%94) Abundance Scan 2607 (28.974 min): 1505.D (-) m/ z 43 55 69 83 97

5000 111 .... , W A I 125 139 207 28.60 28.80 29.00 29.20 29.40 I ■ ‘ I ' 1 ‘dT I ■ ■ ।1 1l .1.) ■ ' i ' ' ' ' i ' ■ ' ■ i ' ‘ ' 1 I ' 1 ' 1 I ‘ ■ i ' ' ' ' i m/z 55.00 96.68% m/z-> Abundance 40 60 80 100 120 140 160 180 200 #60683: Phosphonic acid, dioctadecyl ester 220 240

43 55 69 83 97

5000 T i ■ ■ ' ■ 1 1

111 28.60 28.80 29.00 29.20 29.40 m/z 41.05 95.60%

m/z-> ■ ' i ' ' 40 60 i 1 1 1 ' 1 1 ' 80 >136 __

100 1 i ■ ■ ' ' i ■ ■ ■ 1 i ■ ' ' ■ i ' ■ ' ■ i ■ ■ ■ • i ■ ' 1 ■ i ■ 1 ■ ■ i ' ■ ' ■ i 120 140 160 180 200 220 240 Abundance 43 55 69 83 97 A 28.60 28.80 29.00 29.20 29.40 5000 m/z 82.95 90.30% 111 125 224 252 ■'। ■ i ■ ■ ■ ‘ i ■ ........... । । ।। । (। । m/z-_ . 40.. 60___ 80 100 120__ 140 160 180 200 220 240____ Abundance #40236: 1-Nonadecanol 55 28.60 28.80 29.00 29.20 29.40 83 69 97 m/z 69.00 87.18% 5000- 111 31 42 II, | 125 238 * ' • ■ i ' ■ ■ ■ 1 ■ ' i ' ' ‘ ' i ' ' ' 1 i ' ■ ' ■ i ' ' ■ ■ i ■ 1 ' ■ i ' ' ' ' i m/z-> 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20 29.40

1505.D GCMS0208.M Tue Feb 26 15:14:51 2002 Page 2

NYC-WTC_000003689