GCMS calibration table for method GCMS0412, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Octadecanoic acid Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 29.71 0.72 ug/1 83969 Chrysene-dl2 33.66 Hit# Of 5 Tentative ID MW MolForm CAS# Qual @ 1 Octadecanoic acid 284 C18H36O2 000057-11-4 2 Hexadecanoic acid 256 C16H32O2 000057-10-3 3 Heptadecanoic acid 270 C17H34O2 000506-12-7 58 4 Tetradecanoic acid 228 C14H28O2 _____ 000544-63-8 58 Abundance Scan 2687 (29.713 min): 8016.D (-) m/z 43.00 100.00% 43 A 57 73

5000 129 85 97 | i | i i I i । i— । i r । i i i ; r i i i | 185 284 —1 l4n __ 115 I 1 ■ ' 1 1 143 157 171 1991 241I —L m/z 41.05 29.40 29.60 29.80 30.00 80.45% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72363: Octadecanoic acid 43 60 73 —

5000 129 29.40 29.60 29.80 30.00 85 m/z 73.00 79.62% 97 241 284 I 111 171 185 m/z-> 1 ■ i ■ • 40 60 80 I I > ■ i > ■ 1 > i ■ • > > । ■ . ■ ■ । 100 120 140 160 ■ i ■ ■ ■ > । 180 200 222 | ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । ■ 220 240 260 —280L Abundance #71609: Hexadecanoic acid 43 60 73 A AAAAAM/ I I I I I I I I I I I

29.40 29.60 29.80 30.00 5000 m/ z 57.00 79.22% 129 85 97 256

1 । । ■ • II 1 157 171 185 199 213227 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 73 #72013: Heptadecanoic acid MrMA ।IA/I ■ < ■ Awwwy i ■ ■ ■ > । ■ > • > । 29.40 29.60 29.80 30 00 60 m/z 59.95 75.25%

5000 129 85 97 115 227 - 171 185 I 270 hit Woopeais m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 29.40 29.60 29.80 30.00

8016.D GCMS0412.M Tue Apr 16 12:08:08 2002 Page 5

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