GCMS results sample AE05749, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI702\5749.D Vial: 19 Acq On : 18 Apr 2002 1:47 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Octadecanoic acid, 2-methylpro Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 32.10 0.52 ug/1 71886 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecanoic acid, 2-methylpropyl e 340 C22H4402 000646-13-9 93 2 Butyl tetradecanoate (myristate) 284 C18H3602 000000-00-0 64 3 Octadecanoic acid, butyl ester 340 C22H4402 000123-95-5 58 4 Docosanoic acid 340 C22H4402 000112-85-6 38 Abundance Scan 2947 (32.096 min): 5749.D (-) m/ z 56.00 100.00% 55

5000 41 73 129 285 ■ ‘ 1

—Hr - 441 ■' i'111185 207 241 L 340355 149 267 TIPPWTIWTTTTTT m/z 31.80 32.00 32.20 32.40 57.00 59.08% 1" " i1'111" ■11" ■r i' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000 ........ /V wA .. i i । i ’ II । ii i i । i I i । । r i t r

31.80 32.00 32.20 32.40 285 m/ z 43.05 52.23% 267 J ‘11" 73I97 +4+ • • • I''1 11' 129 185 1 r ■ ■ ■ i " ■r r ■ ■ ‘ i1' " i " " i " ‘' I ■ 241 U 340 " i " " i " " I " " i ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55 A A AA 31.80 32.00 32.20 32.40 / UUA . I ' 1 ' 1 I I ' I ' ' ' <

5000 m/ Z 41.05 50.28% 229 73 211 101 129 185 284 - ’ I’’ I I I I [ I I I I | I r I I | < I I । | i | i | | i | | i | i | i r | Pui v /z->_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ,........ / VA Art A Abundance #73570: Octadecanoic acid, butyl ester ' ' ' I 1 ' 1 ' I ' ' 1 1 1 1,1 1 1’ 1 1 ' 55 31.80 32.00 32.20 32.40 m/ z 55.00 39.25%

5000 285 340 73

.... I YN , , 129 267

m/z-> 1' I'1 , 97 - 4 13’1’1111101-TTTTTCTETTT’E1tH1E31—EIIT1TTTTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 TIFT 185 I 241 i I 31.80 32.00 32.20 32.40

5749.D GCMS0412.M Thu Apr 18 14:10:34 2002 Page 2

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