GCMS results sample AE05749, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1702\5749.D Vial: 19 Acq On : 18 Apr 2002 1:47 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHOES\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Trimethylsilyloxystearic aci Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.90 0.90 ug/1 123487 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 25 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 20 3 3-Isopropoxy71,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 4 1,1,1,5,7,7 -Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 Abundance Scan 3252 (34.896 min): 5749.D (-) m/ z 73.00 100.00% 73

147 5000 221 281 355 429 1 1 r 11 r‘ । 1 ' 1 1 rTi-'-i । ।-I 34.60 34.80 35.00 35.20

n/z-> 50 , 100 117.. . , 150 191U 1 r253,, TTT 200 250 15 1 300 —14 l‘l 327, 350 400 450 500 550 m/z 147.00 51.29% Abundance #56734: 3-Trimethylsilyloxystearic acid, trimethylsilyl est 73

5000 147 233 4 34.60 34.80 35.00 35.20 313 429 m/z 221.05 40.20% 189

m/z-> ■ ■ i • ■ < ■ i > • 50 100 -4 250 300i 339350 387400 I 450 500 550 150 200 Abundance #58871:1 -Monolinoleoylglycerol trimethylsilyl ether 73 ................ /.............. ' ' I ' ' 1 1 I ‘ 1 ' 1 I ' 1 1 1 I ' 1

207 34.60 34.80 35.00 35.20 5000 147 m/z 355.05 28.37% 34 103 , 281

•n/z-> 50 100 .482 . . 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ............ / \.............. । । । r i i i । i i i t । r i i i j r r 73 34.60 34.80 35.00 35.20 m/z 281.00 25.89% 5000 147

/z—> _150 200271250 21327 1 ■ i 1 - 1 > i 50 100 415 519 561 1 ■ • ■ i ■ ■ 1 ■ i ■ ■ ■ ■ i - ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i । 300 350 400 450 500 550 । ■ “i । ' I । ।

34.60 34.80 35.00 35.20

5749.D GCMS0412.M Thu Apr 18 14:10:35 2002 Page 3 NYC-WTC_000047996