GCMS calibration table for method GCMS0412, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Hexadecanoic acid Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

27.34 0.48 ug/1 80803 Phenanthrene-dl0 25.61 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid 256 C16H3202 000057-10-3 (94 2 Tridecanoic acid 214 C13H2602 000638-53-9 72 3 Pentadecanoic acid 242 C15H30O2 001002-84-2 72 4 Tetradecanoic acid 228 C14H28O2 000544-63-8 68 Abundance Scan 2429 (27.345 min): 8016.D (-) m/ z 73.00 100.00% 60 73 43

5000 129 85 97 / TMAA

m/z—> m, 20 40 60 — 80 -4—— 100 111

120 143 177 171 185 199 | 140 160 180 200 213

220 240 256

260 27.00 27.20 27.40 27.60 m/ Z 60.05 84.61% T' 1 ' 1 I

Abundance #71609: Hexadecanoic acid 43 60 73

5000 129 27.00 27.20 27.40 27.60

. J_ 85 97 256 m/z 43.05 75.13%

i 1 ' ‘ ’ i ■ ■ 11 157 171 185 199 213 227 1 ' i ' 1 ■ ■ I ■ ' ' 1 I 1 1 ' ' i 1 ■ ■ ■ i 1 ■ ■ ' i ' ' 1 ■ i ■ ■ ' 1 i ■ ' ' ' i ' ■ Tit m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #70343: Tridecanoic acid 60 73 I I I I I I I I 118" I I I I I I I I I I I I

27.00 27.20 27.40 27.60 5000 m/ Z 41.05 65.82% 129 27 85 i- 97 143 157 , 171| 185 214 | i ■ ' ' ' i ' ■ r ■11 । "I 11-1111 > । । m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #71237: Pentadecanoic acid I 1 ' ' ' I ' 60 7 3 27.00 27.20 27.40 27.60 m/z 55.00 56.79%

5000

42 129 242 85 97

/z—> i ' ' 1 1 11 1 ' 20 40 60 1 11d 1 1 1 1 11 80 100 171 185 I ■ i > ■ > ■ i ■ • • ■ r ■ • 120 140 160 199 > i ■ ■ > ■ । 180 200 > 1 I ■ ■ > ■ । 220 240 ■ '1 rr 260 _ Alm , A 27.00 27.20 27.40 27.60

8016.D GCMS0412.M Tue Apr 16 12:08:07 2002 Page 4

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