DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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Data File : C:\MSDCHEM\1\5973N\02FEB27\02454.D Vial: 5 Acq On : 27 Feb 2002 6:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 11 1,2-Benzenedicarboxylic aci... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

31.11 0.06 ug/L 49090 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 43 2 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 000117-84-0 37 3 (IS*,2R*,5R*,7S*)-2,4-Dimethyl-7... 168 C10H16O2 091926-28-2 33 4 4-Pyridinecarboxaldehyde, 3-hydr... 167 C8H9NO3 000066-72-8 9 Abundance Scan 2457 (31.111 min): 02454.D (-) m/z 149.00 100.00% 149

5000 57 167 236 A............... 86 1'13 208 1 1 1 1 ' * 11 1 1 1 ‘+1++I 30.80 31.00 31.20 31.40 0 1’11111011110111111221111111011110 ’"’1"7"1T 1 1 p 1 1111—1000001-T m/z 167.00 40.39% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326922:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149

5000 57 30.80 31.00 31.20 31.40 167 m/z 57.10 40.36% 0 |......... ........................... 390 " p " 1 p " ' p " ' p ‘" p 1" i11" p " ' p' ‘ ■ p 111 p "' p 1" r " 11 " " r " 11" " 1" " r " 11 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326898:1,2-Benzenedicarboxylic acid, dioctyl ester (CAS)... 149

30.80 31.00 31.20 31.40 5000 m/z 43.10 31.38% 57 167 /

0 390 p " ' P '11 p ' " I p "11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #70509: (1 S*,2R*,5R*,7S*)-2,4-Dimethyl-7-ethyl-6,8-dioxabi... ' ' i 1 ■ ■ 1 i ' ■ ' i ■ ■ ' ■ i 1 ' 149 30.80 31.00 31.20 31.40 m/ Z 55.10 29.59%

5000 167

71 113

0 — TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30.80 31.00 31.20 31.40

02454.D HP022102.M Thu Feb 28 08:47:34 2002 Page 13

NYC-WTC_000005102

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NYC-WTC_000005102Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999