GCMS analysis results for sample AE00472, Feb 26 2002

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•Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.14 ug/L 94749 Chrysene-dl2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, 3-... 211 C8H5NO6 000603-11-2 50 2 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 45 3 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 45 4 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 43 Abundance Scan 2428 (31.094 min): 00472A.D (-) m/z 149.00 100.00% 149

5000 57 71 167 W 43 11 ■ 1 • ' > < i ‘ 1" — 0 84

80 104 120

100 120 140 I 160 180 207 240 ■ i ' ■ ' ' i ' ■ ■ ' I ' 200 220 240 m/z 30.80 31.00 31.20 31.40 71.10 24.71% mlz-> 40 60 Abundance #131213:1,2-Benzenedicarboxylic acid, 3-nitro- (CAS) $$ 3... 149

5000 167 1 1 ■ i ■ 1 30.80 31.00 31.20 31.40 71 m/z 167.00 23.80% | 83 113 0, , । , ,ill, -h- -=-1-4444 132 1 1 1 1 1 40 60 80 100 120 140 160 180 200 220 240 Abundance #326955: Phthalic acid, diisooctyl ester $$ 1,2-Benzenedic... 149 30,80 31.00 31.20 31.40 5000 m/z 57.10 23.38% 57 167 71 | 83vertrlppr 1 1,14,, — 113 0 Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #326921:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... ‘II T 149 30.80 31.00 31.20 31.40 m/z 70.10 16.55%

5000 57 167 71 83 — 113 ,474 0T — ■1 -1 11 1 1 T | l l fl | I /z--> 40 60 80 100 120 140 160 180 200 220 240 30.80 31.00 31.20 31.40

00472A.D HP020702.M Thu Feb 21 09:57:56 2002 Page 15

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