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GCMS analysis results for sample AE00472, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00472, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052271–000052290

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052288
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NYC 9/11 Public Portal Document Library searen Loupur

-Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 1,2-Benzenedicarboxylic aci... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

24.85 0.07 ug/L 51117 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000084-78-6 83 2 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 83 3 Dibutyl phthalate 278 C16H2204 000084-74-2 83 4 Dibutyl phthalate 278 C16H2204 000084-74-2 83 Abundance Scan 1881 (24,849 min). 00472A.D (-) m/z 149.00 100.00% 149

5000 1444 41 56 76 93 105 121 . 205 223 24 60 24.80 25 00 25.20

m/z-> 0— L ----- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 m/z 150.10 A 8.34%

Abundance #284876:1,2-Benzenedicarboxylic acid, butyl octyl ester 149

5000 ■ > । ■ > • ■ । T T 24.60 24.80 25.00 25.20 m/z41.10 8.26%

m/z-> 0TT 42.7776— 194 121— 192205 223 261‘‘330 1*00130—02m—1t3*0———*0nut 20 40 60 80 100 120 140 160 180 200 220 240 260 280 279 ‘r Abundance #223248:1,2-Benzenedicarboxylic acid, dibutyl ester (CAS)... 149 i 1 ■ ■ ‘ 1 1 1 24.60 24.80 25.00 25.20 5000 m/z 56.10 7.03%

41 56 76 104 . 205 223 OTTT -------- /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223232: Dibutyl phthalate T T T T 149 24.60 24.80 25.00 25.20 m/z 223.10 5.15%

5000

29 41 57 76 104 121 163 178 295 223 0′1 ■ dovn 1 Prei) , r trnmte 11117 1 ’ i ' 1 1 11 1 ' 1 ' I ' ' ' ' i' ' 1 ' 1 1 1 1 1 I 1 1 1 1 I ■ ' i ' ■ 1 1 i T /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

00472A.D HP020702.M Thu Feb 21 09:57:55 2002 Page 14

NYC-WTC_000052288

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NYC-WTC_000052288Source: NYC Law Department, mirrored locally

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