GCMS analysis results for sample AE00472, Feb 26 2002

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- Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 DECADEUTERO PHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.47 ug/L 331994 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 86 3 Anthracene-D10 188 C14D10 000000-00-0 86 4 Phenanthrene-diO 188 C14D10 001517-22-2 86 Abundance Scan 1699 (22.771 min): 0O472A.D (-) m/z 188.10 100.00% 188

5000

80 94

—HP —l— 158 22.40 22.60 22.80 23.00 23.20 40 54 66 132 0 InPIPIT — 1 ’1'11 P m/z94.10 18.88% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 TT T T T TiT 22.40 22.60 22.80 23.00 23.20 80 94 m/z80.10 15.46% 66 158 — 0- j ‘‘‘I ‘ ‘‘ p ‘ ‘T -i p PTITT* < 111111 >. । 1 -HTP n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 ___________ 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.15 14.96% N 80 94 160 66 /z-> 0 L, i" " i1r1"1 r1 r’ n - 4-n= r r ■ I ■ ■ > ■)11 •111 > 1111

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 TI 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 11.14%

5000 80 94 66 160 । .......................... .......................... 0 ' I ""T" 11 " I' I’ T T 1T MHHmm TTunr n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 40 22.60 22.80 23.00 23.20

00472A.D HP020702.M Thu Feb 21 09:57:55 2002 Page 13

N YC-WT C_000052287