GCMS analysis results for sample AE00472, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00472, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052271–000052290

Folder label: “GCMS X 1/11/02 A 2/7/02”

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NYC 9/11 Public Portal Document

Library Searcn compound nepo.

. Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 97548 Phenanthrene-dl0 22.63

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC .. 192 C11H12O3 019169-94-9 72 2 2,4-Diamino-6-(hydroxymethyl)pte ... 192 C7H8N60 000945-24-4 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 Abundance Scan 1656 (22.280 min): 00472A.D (-) m/z 192.10 100.00% 192

5000

96 146 T 160 22.00 22.20 22.40 22.60 0 44 i111' I 70 82 THFTH । ■ 111<j b.''j. ।i j j।.11. >Ti11 — TP m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 14—— m/z 96.10 18.56% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 T T T 22.00 22.20 22.40 22.60 146 175 m/z 191.10 16.27%

n/z-> 0 p > > > 11' 1 n > u 1'1 ■ ‘ ।| TTIT i1"' I ■1 ■ ■ i11 ■111 ’ ' i'" ■ r 1 ■ ■ i ■ Arun 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u Abundance #102009: 2.4-Diamino-6-(hydroxymethyl)pteridine $$ 6-Pteri... 163 192

22.00 22.20 22.40 22.60 5000 m/z 146.10 15.77%

66 146 176

0 i ■” 'I" " I ‘1" r ■ TT r 44 121 134 p i . i p i. i! i r. 11 ‘ ‘1′1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline .... A 1 1 i 1111i11 1 ' i 192 22.00 22.20 22.40 22.60 m/z 193.10 13.99%

5000' 82

54 110 30 94 160 i 11| 1111 111 । i p ni-j-i.. . । i . 11. . 1‘ 0 ■ i ■' ’111 1111 ■111"1 ■ I "I'll.!... —T /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 2200 22.20 22.40 22.60

00472A.D HP020702.M Thu Feb 21 09:57:55 2002 Page 12

NYC-WTC_000052286

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NYC-WTC_000052286Source: NYC Law Department, mirrored locally

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