GCMS analysis results for sample AE00472, Feb 26 2002

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.Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1-(2-methoxypro... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.21 ug/L 94347 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy) .. . 148 C7H16O3 013429-07-7 72 2 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 3 2,4-Pentanediol, 2-methyl- (CAS)... 118 C6H14O2 000107-41-5 9

C 4 3-Octanol (CAS) $$ n-Octan-3-ol ... 130 C8H180 000589-98-0 9 Abundance Scan 567 (9.847 min): 00472A.D (-) m/z 59.10 100.00% 59

5000

45 73 0 .1 84 ... 104.. m/z 960 980 45.10 10.00 10.20 14.39% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxy propoxy)- $$ 1-(2-Methoxyp... 59

5000 T 9.60 9.80 10.00 10.20 m/Z41.10 9.04% 31 45 73 194 1 30 miz-> 0 ........... 1........ 'I',I............ ,., TTnr*—o*1‘——u‘——r‘T‘r

Abundance

5000 20 30

31 40 50 60 70 80 90 100 110 120 130 #9591:3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... 59 —

m/z Wh 9.60 9.80 73.10 10.00 10.20 9.00% 73 42 84 0 podoer dlrp H+ n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 #17790: 2,4-Pentanediol, 2-methyl- (CAS) $$ 2-Methyl-2,4-p... 59 130 _AA 9.60 9.80 10.00 10.20 m/z 42.10 8.66% 43 5000

n/z-> 0 - 20 30 40 50 60 .... /..... T........... 70 80 90 100 110 120 130 —A-A 9.60 9.80 10.00 10.20

00472A.D HP020702.M Thu Feb 21 09:57:55 2002 Page 11

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