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GCMS blank analysis results for volatile organics, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.

NYC-WTC_000023409–000023423

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051302\0506LB.D Vial: 6 Acq On : 13 May 2002 3:33 pm Operator: Mc.lean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.25 ug/L 305923 Phe nanthranene-dlO 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual A 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 45 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 45 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 45 Abundance Scan 3319 (22.580 min): 0506LB.D (-3312) (-) m/z 192.10 100.00% 192

5000 .. ................... ...............................

42 0 H" i h. . r ' 70 82 96 120 | u I I | 1 I H | 11 । I | I I I ' | I ■ " ! " ' I | ‘‘|11II| 146 160...... ,| | ' I | i'l I । ‘ | ‘ ‘ H > " ' | 22.20 22.40 22.60 22.80 23.00 m/z 191.10 19.02% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 19/2

5000 ' 1 1 ' 1 1 1 1 1 18i8 TI7 22.20 22.40 22.60 22.80 23.00 m/z 193.10 15.12% 96 165 i i 29 39 51 63 74 83 1 115 126 139 152 1 176 , | 0 ।|1'■'| । 1 l'| ' ‘ " |'I । | 1'1 1 1 | I ' l’i rl ! 1U l ; . . , . । , , . . । . 1 . ( . i . ['I . . i | .'ih . | . ill | 1 1 1111 " i" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81041: Phenanthrene, 3-methyl- / 192 1171, . । । । > |-r-r ‘I7 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.00 14.88%

96 JP 27 39 51 63 82 j| 115 126 139 152 190 176 O' TIWTTWTT)TTTTTTTTTummttmurt H m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 192 ..... 4 22.20 22.40 22.60 22.80 23.00 m/z 96.00 11.00%

5000

96 27 39 51 63 82 ,| 115 126 139 152 165 176 0: TIWTTIWTTTmTTTgTTT 11dAA1adda(eocdscas+mata*et 223107 ' i ' ■ ‘ 1 i ' ‘ * i ' ■ ' ■ i ' ■ diB m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

0506LB.D 050102.M Tue May 14 11:31:59 2002 Page 8

NYC-WTC_000023419

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NYC-WTC_000023419Source: NYC Law Department, mirrored locally

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