GCMS unknown compound analysis, sample AE05303, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\031702\5303.D Vial: 6 Acq On 17 Mar 2002 12:53 pm Operator: McLean Sample 3/11/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ***★*★*★*★★****★★**★****★★*★★****★★*****★**★********★★★★*★***★***★*★★ Peak Number 3 dl-2-Ethylhexyl chloroforma... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

30.61 1.48 ug/L 653373 Chrysene-dl2 30.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 dl-2-Ethylhexyl chloroformate $$... 192 C9H17C1O2 024468-13-1 80 2 LAURIC ACID, N-OCTYL ESTER $$ LA... 312 C20H40O2 000000-00-0 78 3 DI(2 -ETHYLHEXYL) MALONATE 328 C19H36O4 000000-00-0 47 4 oct-3-ene $$ 3-Octene (CAS) 112 C8H16 _______ 000592-98-3 47 Abundance Scan 3036 (30.613 min): 5303.D (-) m/z 57.10 100.00% 57

112 5000 83 239oce 30.20 30.40 30.60 30.80 31.00

Tl/Z-> 0 ..........Hi.A.1. 2^L25LJ85213|T 20 40 60 80 100 120 140 160 180 200 220 24j0 260 280 300 m/z 112.20 53.22%

Abundance ' ■ #102311: dl-2-Ethylhexyl chloroformateS^EthylhexyTchT... “ 57 112

5000 i T^ 83 30.20 30.40 30.60 30.80 31.00 m/z 70.10 48.08%

1 129 149 192 0 P”" ' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance#263373: LAURIC ACID, N-OCTYL ESTERIS LAURTnSAEURE. OCTY. 57

30.20 30.40 30.60 30.80 31.00 5000 m/z 71.10 45.97% 112 83 161 183 201 129 i J 227 255 312 0 I ■ ■" I" " I" " I" '' I" " I" " I' I "'' I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance c7 #279110: DI(2-ETHYLHEXYL) MALONATE I 30.20 30.40 30.60 30.80 31.00 m/z 55.10 41.93%

5000 83 112

0 ■n" 181 199217 238 271 " r " ’ i' " j' "' I'" ' I'' " I Tl/Z-> 20 40 60 80 100 120 1^160 180 200 220 240 260 280 300 30.20 30.40 30.60 30.80 31.00

'5303.D 5080302.M Fri Mar 22 09:42:48 2002 Page 5

NYC-WTC_000059469