GCMS scan report for sample AE05909, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

- Data File : C:\MSDCHEM\1\DATA\031702\5909.D Vial: 21 Acq On : 18 Mar 2002 2:45 am Operator: McLean Sample : 3/14/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 dl-2-Ethylhexyl chloroforma... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

30.61 2.72 ug/L • 11182 80 Chrysene-dl2 30.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 dl-2-Ethylhexyl hloroformate $$••• 192 C9H17C1O2 024468-13-1 72 2 oct-4-ene $$ 4-’ ctene (CAS) 112 C8H16 000592-99-4 49 3 2-Octene (CAS) $$ oct-2-ene $$ 0... 112 C8H16 000111-67-1 47 4 Propanedioic acid, hexyl-, dieth... 244 C13H2404 005398-10-7 47 Abundance Scan 3036 (30.613 min): 5909.D (-) m/z 57.10 100.00% 57

112 71 5000

— । TWTTRTTT i 84 30.20 30.40 30.60 30.80 31.00 I I 97 .. 239 256 OA^ —444— l— 129 143 157 171 185 213 _ IL, m/z 112.20 56.52% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #102311: dl-2-Ethylhexyl chloroformate $$ 2-Ethylhexyl chi... 57 70 112

5000 A... . i ■ ' ■ ■ i ■ ■ r-TT-r-r 43 83 30.20 30.40 30.60 30.80 31.00 m/z 71.10 50.25%

। 97 129 149 192 0- । । " । i° 1 u 4 + । 1 TTTTIWTTIIIg m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #13975: oct-4-ene $$ 4-Octene (CAS) 1 2

_ / i ' '" ' i ' ' ' ■ i ‘ ' 30.20 30.40 30.60 30.80 31.00 m/z 70.10 49.61% 5000

70 1 56 83 42 I . Il 97 0-■ ■ i ■1 ■ ■ i ■ " ■ i1 ' I ’''11 ’ ’ ’' I ’' * ’ I ' ' ' * I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #13735: 2-Octene (CAS) $$ oct-2-ene $$ OCTENE-2 $$ 2-Octen... 1 2 30.20 30020 30.60 30.80 37.00 m/z 55.10 40.23%

5000 70 56 83 42 0-— -AP P— m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 30.20 30.40 30.60 30.80 31.00

5909.D 5080302.M Wed Mar 20 11:30:51 2002 Page 3

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