GCMS scan comments for sample AE06051, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040502\6051.D vial: 10 Acg On 6 Apr 2002 3:48 am Operator: Bohlk Sample SAMPLE 6051 3/15/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ******************************************** * * *********************** Peak Number 1 dl-2-Ethylhexyl chloroforma... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

30.55 1.21 ug/L 654099 Chrysene-dl2 30.24

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 dl-2-Ethylhexyl chloroformate $$... 192 C9H17C1O2 024468-13-1 80 2 1-Octene (CAS) $$ Caprylene $$ n... 112 C8H16 000111-66-0 43 3 Dodecane, 1-fluoro- $$ Dodecyl f... 188 C12H25F 000334-68-9 43 4 Decane, 5,6-dipropyl- 226 C16H34 _____ 119209-20-0 38 Abundance Scan 4676 (30.553 min): 6051 .D (-) m/z 57.10 100.00% 57

71 112 5000 43

129 I 149.... 213226 239 , IVK. 30.20 30.40 30.60 30.80 0 m/z 71.20 59.86% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #102311: dl-2-Ethylhexyl chloroformafe $5 2-Ethylhexyl chi... 57 112 70

5000 43 83 30.20 30.40 30.60 30.80 m/z 112.10 58.70% 97 129 149 0 192 rrm-r ' I ' ' ' ' I''''' I ' "n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #13725:1-Octene (CAS) SS Caprylene $S n-1-Octene SS .alph... 112

30.20 30.40 30.60 30.80 70 5000 m/z 70.10 57.24%

56 83 (I 42 97 0^ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #98264: Dodecane, 1-fluoro- $$ Dodecyl fluoride $$ n-Dodec... 57 30.20 30.40 30.60 30.80 m/z 43.20 41.75%

5000 71

85

0 I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 30.20 30.40 30.60 30.80

5051.D 5080402.M Mon Apr 08 12:13:13 2002 Page 3

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