GCMS data file for sample AE05903, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . 4 . Data File : C:\MSDCHEM\1\DATA\031702\5909.D Vial: 21 Acq On : 18 Mar 2002 2:45 am Operator: McLean Sample : 3/14/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 dl-2-Ethylhexyl chloroforma. . . Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

30.61 2.72 ug/L 1118280 Chrysene-dl2 30.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 dl-2-Ethylhexyl chloroformate $$... 192 C9H17C102 024468-13-1 72 2 oct-4-ene $$ 4-Octene (CAS) 112 C8H16 000592-99-4 49 3 2-Octene (CAS) S$ oct-2-ene $$ O... 112 C8H16 000111-67-1 47 4 Propanedioic a Id, hexyl-, dieth... 244 C13H2404 005398-10-7 47 Abundance Scan 3036 (30.613 min): 5909.D (-) m/z 57.10 100.00% 57

112 71 5000

TTTTT 239 256 30.20 30.40 30.60 30.80 31.00

m/z—> 0- ' ' ■i —129 143 157 171185 unpenTgT 40 60 80 100 120 140 160 180 200 220 240 260 213 XL m/z 112.20 56.52%

Abundance #102311: dl-2-Ethylhexyl chloroformate $$ 2-Ethylhexyl chi... 57 112 70

5000 A.. - 43 83 30.20 30.40 30.60 30.80 31.00 m/z 71.10 50.25% 97 129 1491 192 0- T-p "T TT 11111 ■ i ■1 ■ ■ i ■11 ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■ ■11' ■ m/z— > 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #13975: oct-4-ene SS 4-Octene (CAS) 1 2

30.20 30.40 30.60 30.80 31.00 5000 m/z 70.10 49.61%

70 56 83 42 1 Il 97 0 "It T T ■ I ■ 1 b ■ p TT T T T T m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #13735: 2-Octene (CAS) $$ oct-2-ene $$ OCTENE-2 $$ 2-Octen... 1 2 TAT rT T 30.20 30.40 30.60 30.80 31.00 m/z 55.10 40.23%

5000 70 56 83

m/z-> 42 0- ’TT 40 60 +97 80 ■ i ■ ■ ■ ■ i < ■ ■ • । ■ i ■ ■ ■ ■ i ■ ■ ■ ■ ।

100 120 140 160 180 200 220 240 260 ' i ■ ■ ■ ■ i ■ ■ TPT —et T 30.20 30.40 30.60 30.80 31.00

5909.D 5080302.M Wed Mar 20 11:30:51 2002 Page 3

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