GCMS analysis results for sample AE09571, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.

NYC-WTC_000023023–000023054

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On : 9 May 2002 8:10 pm Operator: Mclean Sample : 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 2-Iodoethyl laurate Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.39 2.19 ug/L 3808000 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Iodoethyl laurate 354 C14H27IO2 1000117-50-2 22 2 Phenol, 2-(2-benzothiazolyl)- 227 C13H9NOS 003411-95-8 3 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 4 4 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20 14 Abundance Scan 4818 (31.388 min): 9570.D (-4811) (-) m/z 227.20 1 .00% 149 227

5000 57 113 167 41 83 [ ,TWAAAAM, . I. Il til . '11 'l" " i1111 r 1'' i1 " ' i " " i ■11 ■ i ■ 31.00 31.20 31.40 31.60 31.80 0+ 1' i " >■ I' ‘‘t «n r ।. 11 m/ z 14 9.0 0 82.88% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #89029:2-lodoethyl laurate 227 43 155 5000 3100 31.20 31.40 31.60 31.80 m/z 57.10 35.29%

„oomow"n4 71 97 183200 m/z-> 0 -25. — — 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 TPWTTTTTUITTTWTWTTTTTTT 354

Abundance #127060: Phenol, 2-(2-benzothiazolyl)- 227

3100 31.20 31.40 31.60 31.80 5000 199 m/z 71.10 35.05%

39 0+ 15—++44444l+441 69 । 1127. — 86 108 154 173 , - 111‘011111111101110TT0-02-1021177 jadno""yy m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #66787: Phthalic acid, diisooctyl ester 149 31.00 31.20 31.40 31.60 31.80 m/z 167.00 31.50% 5000- 57 167 t 41 83 113

m/z-> 0 " i" " r1TTI11 ++132. 111 ’ 111111' I i " " I' ■ " i''1' i'' " i' " ' i ‘' r ' " i' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 31.00 31.20 31.40 31.60 31.80

9570.D 050102.M Mon May 13 11:46:48 2002 Page 17

NYC-WTC_000023044

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