GCMS analysis results for sample AE09571, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.

NYC-WTC_000023023–000023054

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 l-Benzoxirene-2,5-dione, 4-. Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 31.04 1.92 ug/L 3340730 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l l-Benzoxirene-2,5-dione, 4-(3-ox... 238 C13H1804 1000196-81-5 1 2 Dodecane, l,l'-oxybis- 354 C24H50O 004542-57-8 10 3 Undecane, 5-cyclohexyl- 238 C17H34 013151-80-9/10 4 5-Hepten-2-one 112 C7H120 006714-00 10 Abundance Scan 4758 (31.035 min): 9570. D (-4748) (-) m/z 57.10 100.00% 57

5000 83 _hdow* 112 152 191 234 LX l Ju .111694—14 1.................... 0-11' " 11 ‘ * - Ur 207 m/z 30.80 31.00 31.20 31.40 83.15 56.91% m/z-> Abundance :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 43 #4531: 1-Benzoxirene-2,5-dione, 4-(3-oxobutyl)perhydro-3,3... WoMMPMalM 5000 30,80 31,00 31.20 31.40 71 97 125 _ 169 m/z 43.10 51.56% 27 153 |

mlz-> Abundance ol—4—lli444441 rf]'! r । rP. r ■195 220 238 r' । ■ ■ ■ ■ । ■ ■ ■ • । * i * • > ■ । • ■ • ■ । ■ ■ • • ।1 • ■ ■ । ■ ■ • ■ । ■ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #16642: Dodecane, 1,1‘-oxybis- WAALAm"" 57 169

30.80 31.00 31.20 31.40 5000 85 m/z 69.10 45.56% 4'

O-P Irr HH 111 I 140 187 I 241 311 354 TT‘ "I[1177110111/1111111110017[PBIB——--I0IETT aow/asdn"Mpp™ m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #16787: Undecane, 5-cyclohexyl- 57 83 30.80 31.00 31.20 31.40

5000 41

111 154 aWen m/ z 55.10 44.74%

0-— 4l— — 1138.1181................................. ! i,,. ।. r, ।, i .. ’ .,, ।, 11.,. 11, i!।, 11111 u 111111111 ■ ।111 mfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.80 31.00 31.20 31.40

9570.D 050102.M Mon May 13 11:46:47 2002 Page 16

NYC-WTC_000023043

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