NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052802\11603.D Vial: 9
Acq On : 28 May 2002 8:49 pm Operator: McLean
Sample : 5/24 ad re-ext Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 19 Isobenzofuran-1,3-dione, 4,... Concentration Rank 15
R.T. EstConc Area Relative to ISTD R.T.
30.92 0.28 ug/L 235999 Chrysene-dl2 30.76
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Isobenzofuran-1,3-dione, 4,5-dim... 208 C10H8O5 001567-56-2 16
2 5-Methyl-2-N-methylaminobenzophe... 239 C15H17N3 039106-76-8 9
3 Monochloromethyl 2-chloroisopent... 184 C6H10C12O2 1000145-41-2
4 5-(Ethoxycarbonylmethylene)cyclo. .. 239 C13H21NO3 1000106-11- 7
Abundance Scan 4738 (30.918 min): 11603.D (-4737) (-) m/z 92.30 100 0%
92 116
36
208 235
106
5000 49
30.60 30.80 31.00 31.20
0- I ■ 1 ‘ ■ i ■ • ' ■ i ■ ■ ‘ ■ i ■ ■ rn/z 115.90 97.46%
m/z-> 40 60 80 100 120 140 160 180 200 220 240
Abundance #84979: Isobenzofuran-1,3-dione, 4,5-dimethoxy-
44 78 2(8
104
135
5000
65
122 163 179 '30.60' 30.80 31.00 31.20 ' ’ ‘
150 m/z 36.10 73.73%
miz->
0- । . ill [ 44 14 L |1 III,t’r
40 60 80 100
.is
120 140 160 180 200 220
I,I--— I,.....
190
240
’ ‘ I ’ ’ 1* I • ‘
Abundance #85156:5-Methyi-2-N-methylaminobenzophenone hydrazone
208
T
30.60 30.80 31.00 31.20
221 239
5000 m/z 234.90 64.83%
77 89
120
193
ft
58 132 145
165 iso ।
0- । III J, ah ii a i — l1 }i|ili L--H,ii l., 1 Pr । th,.. A111all M
niz-> 40 60 80 100 120 140 160 180 200 220 240 -
Abundance #47905: Monochloromethyl 2-chloroisopentanoate
106 30.60 30.80 31.00 31.20
43 55 76 142 m/z 207.90 63.98%
5000
91
119
niz->
0 —4011.,
60 80
i ■ ■ ■ ■ । • ■1 ■ । 1 ■ ■1 । ■' ■ ■ । • ■ ■ 11 ■ • ■ ■ ।' 1 ■ ' । ■ ■1' । ■ ■
100 120 140 160 180 200 220 240
/
1 i 1 1 ' ' i ' ■ ■ ■ i
30.60 30.80 31.00 31.20
11603.D 052202.M Thu May 30 10:38:56 2002 Page 22
NYC-WTC_000013994
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