NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\051402\10981.D Vial: 10
Acq On : 14 May 2002 8:50 pm Operator: Mclean
Sample : 5/10 kb Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
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Peak Number 7 Isobenzofuran-1,3-dione, 4,. Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
31.01 0.43 ug/L 475200 Chrysene-dl2 30.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Isobenzofuran-1,3-dione, 4,5-dim... 208 C10H8O5 001567-56-2 9
2 6-Amino-2-(m-tolyl)-1,3,5-thiadi... 235 C10H9N3S2 094014-50-3 5
3 3-Chlorothiophene 118 C4H3C1S 017249-80-8 5
4 1-Bromopropadiene -1,2 118 C3H3Br 1000222-14-2 4
Abundance Scan 4754 (31.012 min): 10981.D (-4753) (-) m/z 44.10 100.00%!
44 106
118
208 239
5000
30.60 30.80 31.00 31.20 31.40
0- 1' i1 1 111 . . i ■ . . ■ i . . m/ z 106.00 97.57%
rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240
Abundance #84979: Isobenzofuran-1,3-dione, 4,5-dimethoxy-
44 78 208
104
135
। — ।।11111
5000 TI.T
65 163 vs 30.60 30.80 31.00 31.20 31.40
122
m/z 118.00 75.00%
0- ■ ■ i ■ ■ . AL 4 u t— H TI
190
M., 200 220 240
..180 ■ . i . . . ■ i . '
20 40 60 80 100 120 140 160
Abundance #53046: 6-Amino-2-(m-tolyl)-1,3,5-thiadiazine-4-thione
1 8
235 30.60 30.80 31.00 31.20 31.40
5000 m/z 116.10 73.26%l
91
43 65 143
niz- >
0- ' ■ i ■
20 40 60
177/194....
80 100 120
I
140 160
177
180 200
202
29 —
220 240
Abundance #52766: 3-Chlorothiophene i 1 ■ ■ 1 i 1 ■ ■ ' i ' ' ‘ ' i ' '
1 8 30.60 30.80 31.00 31.20 31.40
m/z 207.95 62.15%|
83
5000 45
58 _
0
12
r-n-j-r 321 M,i IIui 69i1 r........................ .... ■ ■ i ■ ...................... ... । । । । TTT TTTTTurtmr
n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 30.60 30.80 31.00 31.20 31.40
10981.D 050102.M Thu May 16 14:37:16 2002 Page 10
NYC-WTC_000023984
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