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GCMS analysis results for sample AE08252, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08252 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047802–000047829

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047822
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08252.D Vial: 10 Acq On : 17 Apr 2002 4:52 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 12 Anthracene-dlO- Concentration Rank 1 R. T. EstConc Area Relative to ISTD R.T.

23.17 0.48 ug/L 722866 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO - 188 C14D10 001719-06-8 91 ( Phenanthrene-diO 188 C14D10 001517-22-2 81 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 47 4 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 42 Abundance Scan 3420 (23 174 min) 08252.D (-3414) (-) m/z 188.10 100.00% 188

5000

94 ) 1 80 22 80 23.00 23.20 23.40 23 60 40 52 66 ,102 132 146 160 0 mPmmmmmmm —TH m/z94.05 19.54% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d10- 188

5000 _ -------------- 22 80 23.00 23 20 23 40 23.60 80 94 m/z 189.10 15.23% 66 160

n/z-> 17 30 42 52 | .1 102 118 132 146 +170.180 0 ' i " " i' " 11' ।■ 11111 111111111111 | " ■ 111 ।11 n ' i'|! । " 111.. 11 r 11111111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Wr

Abundance #79827 Phenanthrene-d10 188 ’ i 1 • ■ ■ i 22 80 23.00 23 20 23.40 23.60 5000 m/z 184.05 14.32%

80 94 160 30 42 52__ 66 11. 102110118 ,. 132 . । 146 . h . 170 189 1 ... 0 ll"llllllllllllllllllllllllllll n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739 Cycloheptanone, 4-phenyH ■ i ■ ■ • 1 i 188 22.80 23 00 23 20 2340 23.60 117 104 m/z 80.05 12.62% 91 160 5000 131 170

27 39 51 65 78 145

n/z-> -44++ r H UiL 0 ryn r i [, i M i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1111" Turr _____ ) 1 ' I 1 ' ' ' I ' i 1 ' ■ 1 1 1 22.80 23.00 23.20 23 40 23.60

08252.D 041702SCAN.M Thu Apr 18 09:14:02 2002 Page 17

NYC-WTC_000047822

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NYC-WTC_000047822Source: NYC Law Department, mirrored locally

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