GCMS analysis results for sample AE08252, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08252.D Vial: 10 Acq On : 17 Apr 2002 4:52 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 13 Acetamide, 2,2,2-trichloro-.. . Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

31.05 0.21 ug/L 264761 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetamide, 2,2,2-trichloro-N-phe. . . 237 C8H6C13NO 002563-97-5 9 2 Propionic acid, 3-[(4-acetyl)phe. . . 235 C12H13NO4 062134-55-8 5 3 Benzenamine, N,N-dimethyl-4-[(3-. . . 239 C15H17N3 000055-80-1 5 4 Pyridine, 3,3(2,4-piperidinedi... 239 C15H17N3 018793-19-6 5 Abundance Scan 4760 (31 047 min): 08252 D (-4759) (-) m/z 40.00 100.00% 40

120 5000 51 207 235 84 106 30.80 31 00 31 20 31 40 t | । | 1 1 _ r 0- ■ ■ i ■ ■ ■ ■ i m/z 119.70 49.43% ti/z--> 40 60 80 100 120 140 160 180 200 220 240 Abundance #120890: Acetamide, 2.2.2-trichloro-N-phenyl- 1 0

5000 ‘ 1 1 ' 1 1 ' | 1 ' ' ' f-r-r 77 30.80 31.00 31.201 31.40 237 m/z50.90 39.02% 65 92 132 166176 189 202 || 40 51 -114119.1, 01 TII+ ,’) - , 1j | I I I | ! I I T' I I -

n/z-> 40 60 180 100 120 140 160 180 200 220 240 Abundance #54151 Propionic acid, 3-[(4-acetyl)phenylaminocarbonyl]- 110

135 30.80 31 00 31.20 31.40 5000 235 m/z 120.60 35.04%

43 55 . 101

n/z-> 0 40 LL 7321,1 60 80 100 120 I 146 162174 140 160 180 202 200 220 P 220 240 Abundance #54 275: Benzenamine, N.N-dimethyl-4-[(3-methylphenyl)azo]- ' ' I ' ' 1 ' I ' 1 1 '0 30.80 31.00 31 20 31.40 m/z 207.10 34.47% 239 5000 77 91 42 65 105 148 0 .1 1 1,521 r । । 11 । । IL — .. 2— . wommnmm* /z-> 40 60 80 100 120 140 160 180 200 220 240 30.80 31.00 31 20 31 40

08252.D 041702SCAN.M Thu Apr 18 09:14:02 2002 Page 18

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