GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 3-Methyl-1-[(1H)-1,2,4-tria. .. Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

28.86 0.23 ug/L 235670 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methyl-1-[(1H)-1,2,4-triazol-l... 153 C7H11N30 064922-02-7 4 2 Z-10-Pentadecen-l-ol 226 C15H30O 1000131-00-6 2 3 3-Methylpenta-1,4-diene-3-ol 98 C6H10O 1000215-36-6 2 4 Acetamide, 2-chloro-N-(2-cyanoet... 146 C5H7C1N2O 017756-81-9 2 Scao 4387 (28 855 mio) 07766 D (-4376) (-) m/z 40.20 100.00% 40

49 111 5000 82 71 I ■ ■ ■ ' i 28 60 28 80 29.00 29.20 95 0- - m/z 43.30 73.03% n/z-> 40 60 80 100 120 140 160 180 200 220 Abundance 43 #6955' 3-MethyH-[(1H)-1,2,4-triazol-1-yl]butan-2-one

83 APwAwklasp 5000 71 TI 28 60 28.80 29.00 29.20 m/z 111.30 56.74% 55 "" — |............. 154.............. 0- — n/z-> Abundance 40

43 60 80 100 120 140 160 #5032 Z-10-Peot86eceo-1-ol 180 200 220 AM i 28.60 28.80 29.00 29.20 55 5000 69 m/ z 49.20 56.46% 83 95 IV

n/z—> 01 .40ll . ll60 lll—80l M, qll, ), 109 120121 136140 149158167 100 160 181 180 199 211 226 200 220 460063006 #6932 3-Methylpenta-1,4-diene-3-ol 43 28 60 28 80 29 00 29.20 m/z36.20 47.19% 5000 83 55 71

/z-> 0 J40 — IpI ,I-I|I ...97 ........... 60 80 100 120 140 160 180 200 220 I "II 28.60 28.80 29.00 29 20

07766.D 041202SCAN.M Tue Apr 16 13:42:10 2002 Page 10

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