GCMS analysis results for sample AE08252, April 2002

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Laboratory report documenting GCMS analysis of sample AE08252 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047802–000047829

Folder label: “GCMS X 4/8/02 A 4/17/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\020417\08252.D Vial: 10 Acq On : 17 Apr 2002 4:52 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 9-Borabicyclo[3.3.1]nonane,... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 22.64 0.31 ug/L 461530 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9-Borabicyclo[3.3.1]nonane, 9-(l... 192 C13H25B 136704-93-3 50 2 Bitoscanate 192 C8H4N2S2 004044-65-9 47 3 2-Propenal, 3 -(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 40 Abundance Scan 3330 (22 645 min). 08252.D (-3322) (-) m/z 192.10 100.00% 15 2

5000

..... ........................................................... 146 160 , 04 TIT T 54 ™ 82 T 118 THH ......... 'I...... ........... . ■ ■' 'F' ■ i'' m/z 191.10 22.40 22.60 22.80 23.00 22.91% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80919: 9-Borabicyclo[3 3 1]nonane, 9-( 1-ethylpropyl)- 19 2

93 121 5000 1 i ' 1 ■ ' i ' ■ ■ i ‘ ■ i 41 67 81 22 40 22 60 22 80 23.00 55 108 27 m/z 193.10 15.91% . 151

~n/z—> 0 Amal— Ap. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80930: Bitoscanate 192

22.40 22.60 22.80 23 00 5000 m/z 146.10 15.58% 134 90 160 — 20 50 63 75 99,107 116 148 0+ ?-HHH#+ "'I'll"........ . ... . 11 ''I'" i''' 11''' " ' i" " t1" ' i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953 2-Propenal, 3-(3,4-dimethoxyphenyl)- .................... A.................. 192 22.40 22 60 22.80 23 00 161 m/z 96.00 14.49%

5000

77 91 121 149 177

L L al,.. .... 52 64 103 138 0 TI‘ . ........... Il TT’T /z- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22 40 22.60 22 80 23 00

08252.D 041702SCAN.M Thu Apr 18 09:14:02 2002 Page 16

NYC-WTC_000047821

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GCMS analysis results for sample AE08251, April 2002 · Box DEP Box 27

NYC-WTC_000047772

Laboratory report documenting GCMS analysis of sample AE08251 conducted on April 19, 2002, including surrogate recovery data.

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