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GCMS blank results for sample AE11282, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for GCMS analysis of sample AE11282 conducted between May 13 and May 16, 2002.

NYC-WTC_000024534–000024542

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Llbrary aearen compound Report

Data File : C:\MSDCHEM\l\DATA\020516\0513LB.D Vial: 4 Acq On : 16 May 2002 12:20 pm Operator: Nefliu Sample : 05/13 lab blk Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.97 0.32 ug/1 26981 Phenanthrene- dl 0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 Anthracene-dl0- 188 C14D10 001719-06-8 38 3 Benzaldehyde, 2,6-difluoro-4-hyd... 188 C8H6F2O3 1000116-28-9 37 4 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 36 Abundance Scan 4917 (31.969 min): 0513LB.D (-4903) (-) m/ z 188.20 100.00% 188

5000

49 66 80 94 J!......... 31.60 31.80 32.00 32.20 32.40 1 124 ■I""।""iu 1111" p■ ।।■ J.।.111' "1 r11,11" " ।"111'1" ।" " ।" "i"i" " ।1 "■ ।111 1’11’1 158 m/z 80.10 29.88% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 1 /........... _ Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 32.40 80 m/z 94.20 19.82% 94 160 30 42 52 66 11 108 118 132 146 II 170179 ''I'"........ .................. 11. .| ■ 11........ ...... —————— TT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

31.60 31.80 32.00 32.20 32.40 5000 m/z 189.20 18.05%

80 94 160 17 30 42 52 66 108118 132 146 , || 170179, 11■■ ■ < । • I *"11''riI'111 l ■|l-l ■■ il 1111111111 111IT I । li 1i11111111 lT|'i 1111111111’l’l TT mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79823: Benzaldehyde, 2,6-difluoro-4-hydroxy-3-methoxy- 188 31.60 31.80 32.00 32.20 32.40 m/z 66.10 15.67% 5000 173 117

m/z—> 411sl7..S4,76.,88,27,106,1128.115155, 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TTT 31.60 31.80 32.00 32.20 32.40

0513LB.D SCAN020507.M Fri May 17 10:30:07 2002 Page 5

NYC-WTC_000024541

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NYC-WTC_000024541Source: NYC Law Department, mirrored locally

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