GCMS analysis page for sample AE11567, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\02052111567.D Vial: 20 Acq On : 22 May 2002 3:08 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Cyclic octaatomic sulfur Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 35.88 0.28 ug/1 24131 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

41 Cyclic, octaatomic sulfur 256 S8 010544-50-0 74 2 Ethyl /Chloride 64 C2H5C1 000075-00-3 4 3 Ethyl /Chloride 64 C2H5C1 000075-00-3 4 4 Ethene, 1,1-difluoro-____ ________64 C2H2F2 000075-38-7 3 Abundance 1 Scan 5583 (35.883 min): 11567. D (-5572) (-) m/z 64.00 100.00% 64

5000 128 96 160 256

m/z-> 0- 44 ............ I ,l | । , , , 1 1 1 1 1 1 1 1 1 1 1 1 I 20 40 60 LA 80 100 1 120 in 140 192 -1. — —1 160 180 200 220 244 ।

240 TBn 260 35.60 35.80 36.00 36.20 m/z 127.90 36.75% Abundance #113565: Cyclic octaatomic sulfur 64

5000 ■ ■ । ■ 35.60 35.80 36.00 36.20 m/z 96.00 21.40% 32 — 96 128 160 192 256

mfz-> 01 ......60 176--4110----44 .....20 140 80 —24H4 100 120 140 160 180 200 220 240 260 Abundance #20621: Ethyl Chloride 28 64 - 35.60 35.80 36.00 36.20 5000 m/z 255.80 19.27% 49

0- ■111 ■I p-r , W I I"1 ■11 * ‘ ' i * * ■ ■ । *1 • ■ । *1 *11 ■11 ■ ।11 *11 *1 1 ■ r1”* • • ।1111111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #107943: Ethyl Chloride 8 35.60 35.80 36.00 36.20 m/z 159.90 17.67% 64 5000

49

0 JU 1 I. . 1l t 1.. ....... 15 I 4. ...... h ■ ■ । ■ rnfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 35.60 35.80 36.00 36.20

11567.D SCAN020521.M Fri May 24 09:41:23 2002 Page 7

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