Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
NYC-WTC_000043806–000043818Folder label: “GCMS X 4/25/02 A 5/7/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C: \MSDCHEM\1\DATA\020507\09769.D Vial: 16 Acq On 8 May 2002 2:55 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 6.13 0.72 ug/1 59501 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual
11 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 78 2 Sulfurous acid, bis(1-methylethy... 166 C6H14O3S 004773-13-1 17 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 9 4 .beta/.-d-Fructofuranose, 1,3,4-t... 288 C12H1608 1000151-08-8 9 Abundance Scan 519 (6.129 min): 09769.D (-512) (-) m/z 43.10 100.00% 4t3
5000
' ‘ I ' 1 ' 1 1 1 1 1 1 1 1 1 1 ' r1 1 1 1 I 5.80 6.00 6.20 6.40 ........... 11137 ''' 49''i 1 1 ' 1 1 631 1 ' ' । '' । ' ।82 • । ' ' 97' ' । ' ■ ■ 110 117 125 । । ' ' । ' । ' i ' ' ' i i i i m/z 125.00 8.57% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877: 2-Propanone, 1,1,1-trichloro- j 43
5000 I A 5.80 6.00 6.20 6.40 m/z 47.00 7.77% 15 27 36 ,49 55 63 76 83 91 97 110 117 125 1 ■ i ' —4+ till’) ' 11 । I’dii । r ii । । i'i'i ‘ I’ ‘ ■ ’ I ' ' ' ' I • ' ‘ ' I ' ' ।, m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4866: Sulfurous acid, bis(1-methylethyl) ester 43 AuuWWAuamyopv 5.80 6.00 6.20 6.40 5000 m/z 82.10 6.15%
27 59 ............. Ij 371 | +TT 51 —LTHr 69i1 I ' ' 77■ ■ i 8,3 91 109 , , , । 125 । , m/z->10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7672: 2-Acetylthiazole IA,... ) , 1A,., I । 1 1 । । 43 5.80 6.00 6.20 6.40 m/ Z 83.00 5.47% 5000 99 127 58 112 85 15 26 32 1 m/z--> TTPTTH 10 20 30 40 +52 50 11 , , ........ , , . npr —— 60 70 80 90 14 । NV. li T A,A,ana AMs 100 110 120 130 5.80 6.00 6.20 6.40
09769.D SCAN020507 .M Tue May 14 08:43:26 2002 Page 4
NYC-WTC_000043813
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NYC-WTC_000043792
Analytical report for sample AE09768 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043779
Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046147
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10132 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046192
Gas chromatography-mass spectrometry analysis of sample AE10135 performed May 17, 2002, detecting unknown compounds and 2,4-DDD surrogate at 96% recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024791
Laboratory report of GCMS analysis for sample AE10242 conducted on May 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024871
Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000043745
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 25 and May 7, 2002.
Filed in the same folder
NYC-WTC_000043746
Fragmented page containing Method 508 headers and partial text from a DEP laboratory record dated April 2002.
Filed in the same folder
NYC-WTC_000043749
Laboratory report documenting a method blank analysis for GC/MS testing of volatile organic compounds from May 2002.
Filed in the same folder
NYC-WTC_000043756
Calibration data report for sample AE09684 listing response factors and concentrations for target analytes in May 2002.
Filed in the same folder
NYC-WTC_000043760
Reference gas chromatography-mass spectrometry analysis with manual result entry for sample AE09684, detecting multiple organic contaminants.
Filed in the same folder