GC/MS analysis results, sample AE09769, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020507\09769.D Vial: 16 Acq On 8 May 2002 2:55 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.65 0.49 ug/1 40182 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 59 3 Acetaldehyde, trichloro- 146 C2HC130 000075-87-6 37 4 Acetaldehyde, trichloro- 146 C2HC130 000075-87-6 32 Abundance Scan 97 (3.649 min): 09769.D (-93) (-) m/z 74.00 100.00% 74

5000 47 — । > । । । । । A MW Pr t । । — । - 3.40 3.60 3.80 4.00 It l l, 110 ... .... ...... 424. . 547 m/z 82.00 52.52% m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #28338: Acetonitrile, dichloro- 74

5000 3.40 3.60 3.80 4.00 47 m/ z 84.00 44.17%

/z-> Abundance 0 12 11 , i 1 ' ■" 1 1

35 50 74 , 108 ■ ।1 ' ‘ 1 । 1 1 ' ■ । 1 ■ ■ 1 । ■ ' ■ ■ । ■ ■ ‘ 1 i 1 1 1 1 i 1 1 1 1 i ' 1 1 1 i 1 1 1 1 i 1 100 150 200 250 300 350 #115342: Acetonitrile, dichloro- 400 450 500 550 MMWMMMy/y

3.40 U 1 ' ' ' 1 1 1 1 ‘ I ' ' 1 1 1 1 1 1 1 I ‘ 1 ' 3.60 3.80 4.00 5000 m/z 47.00 34.42%

m/z-> Abundance 0 50 100 150 200 250 300 350 #116335: Acetaldehyde, trichloro- 400 450 500 550 AA) WAw Wh 1 1 । ' 1 ■ ■ । ■ 1 1 1 I ' 1 ' ' 1 1 ' ' 82 3.40 3.60 3.80 4.00 m/z 76.00 28.51% 29 5000 111

n/z-> 0 <1 Mi 50 100 146

150 200 250 300 350 400 450 500 550 - i 3.40 1 1 —mw . 3.60 3.80 4.00

09769.D SCAN020507 ,M Tue May 14 08:43:23 2002 Page 3

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