GCMS analysis results, sample AE10135, May 2002

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Data File : C:\MSDCHEM\1\DATA\020513\10135.D Vial: 21 Acq On : 14 May 2002 8:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Acetonitrile, dichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.64 0.39 ug/1 31187 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual L Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 53 2 Ace c acid, trichloro-, ethyl e... 190 C4H5C13O2 000515-84-4 25 3 Tri/chloroacetic Acid 162 C2HC13O2 000076-03-9 10 4 Chi oral Hydrate 164 C2H3C1302 000302-17-0 9 Abundance Scan 96 (3.643 min): 10135.D (-93) (-) m/ z 74.00 100.00% 74

5000 47 35 I ' ' ' ' I ' TI T 1 LTMT" I I I | !" ! I 56 3.20 3.40 3.60 3.80 4.00 X 265 1 1 । 1 ' ' ,40I ' 11I,, 59 11 60 ' ' 1I Tlil r i [ r I i I | i । i i | 1 । 1 1 | । 1 1 1 । । । i i । v ■■ I | I I I 1 | । i i i । 11 I m/z 81.90 58.19% /z-> 20 80 100 120 140 160 180 200 220 240 260 Abundance #28338: Acetonitrile, dichloro- 74

MAAAAA_____ AA A_________ 5000 ‘ ' ' 1 | ' 1 V 1 | ‘ 177I । 1TT | 1 1 1 47 3.20 3.40 3 60 3.80 4.00 m/z 84.00 34.10% 35 1,2 I,|| I, 62 । 36 108 /z-> Abundance 1 1 ' 1 1 ' 1.. 1 ' ^ri T1 1 1 T-Jt 20 40 60 80 100 120 140 160 #116280: Acetic acid, trichloro-, ethyl ester 180 200 220 240 260 wvyMwwy YMMWAAW 82 47 i 1 ■ ■ ■ i 1 ■ 1 ■ । ■ 1 1 1 i 1 1 1 1 i 1 1 1 3.20 3.40 3.60 3.80 4.00 5000 117 m/z 76.00 32.84%

63 , , ill . .... .li . , S3 99 129 155 ' 1 i 1 ■ 1 1 r1 1 1 "T*4r । ft I, .1| T 1,141 i i l i 1167 I । ill r । 1 190I ...................... । ।i I । । । । । | । । i । ■ i । । i i I I "I" I I I | I I

/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance 82 #32571: Trichloroacetic Acid .. 3.20 3.40 3.60 +14414 ...... 3.80 4.00 m/z 47.00 31.36% 45 ... 5000

29 63 99 127 4 TdB|1 . 1112.|.................. ' ' I ' ' ' 'T | ' . ! . | | I I | I I I I TT I ( | > < /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 3.20 3.40 3.60 3.80 4.00

10135.D SCAN020507 .M Wed May 15 08:30:27 2002 Page 3

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