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GCMS analysis results for sample AE11154, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.

NYC-WTC_000025542–000025555

Folder label: “GCMS X 5/17/02 A 5/16/02

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Scanned page image, NYC-WTC_000025548
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11154.D Vial: 19 Acq On : 22 May 2002 2:08 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.65 0.35 ug/1 26397 1,4-Dichlorobenzene-d4 11.37

Hit# of 5 Tentative ID MW MolForm CAS# Qual

• 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 43 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 42 3 Acetaldehyde, trichloro- 146 C2HC130 000075-87-6 12 4 2-Amino-4-methyl-4-pentenoic acid 129 C6H11NO2 1000133-00-5 12 Abundance Scan 97 (3.649 min): 11154. D (-93) (-) m/z 74.00 100.00% 74 82 5000 35 47 1 .TP Pi । i । r । । 1 II Of " i11" i1"111 l Ih 1,1 'i " Ti-3 I 55 |,... 108................. 170 m/z 3.40 3.60 81.90 3.80 4.00 55.87% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 ___ 3.40 , J,, AAA-A-AAA 3.60 3.80 __________ 4.00 47 m/z 83.95 39.26% 35 12 26 ....... . 1 108 miz-> Abundance ol TTIIPTTTTTH -rrnI TI 111 ■ ■1111''11" ■11" ■' i'1" i " ■ ■ r ' ■ ■ i1 n 11" 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #115342: Acetonitrile, dichloro- 74 wMWhWWatss 35 3.40 3.60 3.80 4.00 5000 82 m/z 76.05 34.57% 47

ol ‘ 1**1111111111+4—T ‘T '' I " " I " " I " " I " " I " " I " " I " " I " rI I'1 " I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116335: Acetaldehyde, trichloro- 82 3.40 Ap 3.80 4.00 3.60 m/z. 47.05 25.87% 29 5000 47 111

119 t"17.60, — AT,, 60 70 146 0 ■ 111" ■ j ■'''1 qmmmpm TTTTTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.40 3.60 3.80 4.00

11154.D SCAN020521.M Fri May 24 09:23:28 2002 Page 3

NYC-WTC_000025548

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NYC-WTC_000025548Source: NYC Law Department, mirrored locally

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