GCMS sample analysis report AE08483, May 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08482.D Vial: 19 Acq On : 20 Apr 2002 1:51 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.66 0.28 ug/1 385496 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 50 3 Furan, 3-methyl- 82 C5H60 000930-27-8 7 4 Thiirane, methyl- 74 C3H6S 001072-43-1 7 Abundance Scan 99 (3.661 min): 08482.D (-82) (-) m/ z 74.10 100.00% 74 82 5000 47 ... M, ------ 40 88 3.40 3.60 3.80 4.00 n1 ■' i ■ ■ ■ ■ i ■ 1 ' ‘ i ■ ■ ■ ■ i m/z 82.00 53.68% . mfz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 4M - 411m, 4 , , , 3.40 3.60 3.80 4.00 47 35 m/z 84.00 34.51%

n/z-> Abundance 12 I ' ' ' | I ‘ 10 -2.4 ‘ | ‘ 201 30 40 -2-1 ’It , 90 50 60 70 80 #115342: Acetonitrile, dichloro- 74 108 I < l ■ > ' < l » ■ > >’| 100 110 • 4 l

""PMMypkLs... 35 ' ■ i • ■ ■ ' i 1 1 ' 1 1 1 1 1 1 1 1 ' 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 29.71% 47

। hnut i -i 11111 (। "T-1 1 ■ i ■ ■ ■' । ■ ■ ■ • । ‘ । niz-s 10 20 30 40 50 60 70 80 90 100 110 Abundance #32367: Furan, 3-methyl- . 1A । ri 1T| i i 82 3.40 3.60 3.80 4.00 m/z 47.00 22.20% 53 5000 39

28 t, 11 16 n , ll . il|i|h 444 l. 63 69 TO , 45 | MYMMMAMMsmayury T1'1 ITt 1 1 «i > * >' । > * • • । * ■ > * । • - < ■ j • —■ • ir * ■»j > > 111 ■ ।»। n/z-> 10 20 30 40 50 60 70 80 90 100 110 3.40 3.60 3.80 4.00

08482.D SCAN020418.M Thu May 02 11:44:26 2002 Page 3

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