GCMS analysis results for sample AE08488, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08486.D Vial: 23 Acq On : 20 Apr 2002 5:47 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.66 0.37 ug/1 496048 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 9 4 Allyl mercaptan 74 C3H6S 000870-23-5 7 Abundance Scan 99 (3.660 min): 08486.D (-89) (-) m/z 74.00 100.00% 74 82 5000

IFP - 38 47 .... .. 1 ■n-1 . . 88 ■ ‘i * 3.40 3.60 3.80 4.00 ‘I‘l । । ।। । । [ m/z 82.00 56.89% ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 —A TYA . 3.40 3.60 3,80 4.00 47 m/z 84.00 32.12%

n/z-> Abundance Tmnn—m——m— 11 ‘'i।। . 10 20 30 40 50 60 70 #28338: Acetonitrile, dichloro- 74 TBid 80 1 ■ i ■ ■ ■ • i 11 1 1 i ' ‘1 1 i 90 100 110 wAo 82 ' ' 3,40 3.60 3.80 4.00 ‘ 5000 m/z 76.00 30.80% 47 35 12 26 — , 108 . "IB ' • । ■11'1 ■1 ’ i ■1 ■ ■ । niz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312: 3,3-Dichloropropyne 74 T TT ' i r-[ 3.40 3.60 .Arrn.) 3.80 4.00 m/z 47.05 15.91%

W 5000 38 47 AMWWH z—> --21 20 10 40 30 I i 53 60 . 11 . r-r'.'i . n TT 31′4 50 60 70 82 108 ‘ i 1 ■ ■ ‘ I 1 ■ ■ ‘ i ■ ‘ 1 1 i ' ■ 1 1 i 80 90 100 110 * * i * * • * ।' * * * i *1 *11 *1 3.40 3.60 3.80 4.00

08486.D SCAN020418.M Thu May 02 11:56:34 2002 Page 3

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