GCMS analysis results, Sample AE08263, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08263.D Vial: 20 Acq On : 18 Apr 2002 1:07 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

3.59 0.20 ug/L 153108 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 53 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 9 Abundance Scan 87 (3 590 min). 08263 D (-83) (-) m/ z 74.00 100.00% 74

82 5000 40 47 ' i 1 ' 1 ' i ■ —PA 3.80 4 00

n/z-> Abundance 0+ 1 • i ■ ■ ' - i ■ ■ ■ ■ i 10 20 30 aa... 40 50 60 70 88 ■ । > I I । । । ■ ■ 80 90 100 110 3.20 m/ z 3.40 81.85 3.60 55.58% #115342: Acetonitrile, dichloro- 74 35

5000 82 -4 3 20 3.40 4.00 ' 47 m/ z -40.00 33.50% 40— n/z- > 0+ 1 ' i ■ - ■ - i 1 1 - - । 1 1 10 20 30 40 + 50 60 ■ । ■ ■ ■ ■ । • 70 80 1 ' i - - - ■ i ' ■ ■ ■ i - 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 3 20 3.40 3 60 3 80 4 00 5000 82 m/z 76.00 28.85% 47 35 0+ 12 111 I +26, —— . 62..........! ■ i 1 ■ - ■ I ' ,l ■ i ■ ■ ■ ■ i ■ ■ 108 • 1 ’ | ■ ■ ■ ■ l

n/z-> Abundance 10 20 30 40 50

4rt 60 70 #28161: Allyl mercaptan 80

74 90 100 110 . .....4/..... 3 20 3.40 3 60 3.80 4.00 m/ z 47.00 20.98%

5000 MMHWpyAbwke 47

n/z- > 0 -ll ,1,23..59...891 10 20 27 33 30 I 40 50 60 70 1 ' I ' ' ' ' I ' ' ' 1 I ' ' 1 ' I ' ' ' ' I 80 90 100 110 3.20 340 3 60 3 80 4.00

08263.D 041702SCAN.M Thu Apr 18 09:51:12 2002 Page 6

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