GCMS analysis results, Sample AE08269, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08269.D Vial: 25 Acq On : 18 Apr 2002 5:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.68 0.40 ug/L 478608 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 3 Allyl mercaptan 74 C3H6S 000870-23-5 25 4 N-Nitrosodimethylamine 74 C2H6N20 000062-75-9 4 Abundance Scan 102 (3 678 min): 08269 D (-95) (-) m/z 74.00 100.00% 74

82 5000

47 - 39 3.40 3.60 3 80 4.00 - 88 0 1l-,—5860... — 80 ' 1 i ' ■ ■ ' i 1 1 1 ' i ' ' ' ' i m/z 81.90 52.19% Ti/Z—> Abundance 10 20 30 40 !50 70 #28338 Acetonitrile, dichloro- 90 100 110 I 74

5000 82 I P 3.40 3 60 3.80 4.00 47 m/ z i84.00 33.38%

W.. 35

n/z-> 0+ 12 TI—n—- 26,41440 . 62......... , 1 I ' 1 1 1 1 1 . 108 ' ' i ■ ■ ■ ■ i ' 1 1 1 I ■ ' ' ■ i

Abundance 10 20 30 40 50 60 70 80 #.115342: Acetonitrile, dichloro- 90 100 110 WApwp 74 35 340 3 60 3.80 4.00 5000 82 m/z 76.00 30.08% 47 40

T/z- > 01 ■ i 10 ■ ■ ■ ■ i 20 ■ ■ ■ ■ 30 i 1 । IL +— 40 50 60 1 I ' ■ ' 1 1 1 70 I

80 90 100 110 Abundance #28161' Allyl mercaptan 41 74 3.40 3.60 3.80 4.00 m/z 47.00 21.99%

5000

27 33 47

1153.58.44241 W WMo 0 - 1 ■ i ' ' ■ ■ I ■ ' • 1 i ' 1 ' 1 i ■ • ' ' i n/z—> 10 20 30 40 50 60 70 80 90 100 110 3.40 3.60 3 80 4.00

08269.D 041702SCAN.M Thu Apr 18 10:02:26 2002 Page 6

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