GCMS analysis page for sample AE11154 showing unknown compounds and surrogate compound recovery data.
NYC-WTC_000025556–000025567Folder label: “GCMS X 5/17/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11154.D Vial: 20 Acq On : 16 May 2002 6:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.12 0.61 ug/1 45029 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 50 2 4-Pentenoic acid, 2-acetyl-, eth. . . 170 C9H14O3 000610-89-9 9 3 Hexanoic acid, 9-decen-l-yl ester 254 C16H30O2 1000160-13-5 9 4 2-Butanone, 4-chloro-4,4-difluoro- 142 C4H5C1F2O 001515-16-8 9 Abundance Scan 517 (6.117 min): 11154.D (-508) (-) m/z 43.10 100.00% 43
5000
5.80 6.00 6.20 6.40 153 63 73 ..... . ...... .... TTPTTTTTTTTTTTTT 1 "i"1 'T1"1111" i111 ’I’’ "i ’ ’’1’’ "i' ri n111111111111111111111' 111"'111' m/z 47.05 9.37% . /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #3877:2-Propanone, 1,1,1 -trichloro- 43
5000 AAMWMawM/Myuhwsmps 5.80 6.00 6.20 6.40 m/z 127.10 9.16% 15 27 U h,+r । Arll 1,31 63 73 83 97 110 125 1' P "' i"1 ■ i11 ■ ■ ।" ''''111111 ■' tT 111' r 111111' 111''' 111' 1111' 111111111 mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #110318: 4-Pentenoic acid, 2-acetyl-, ethyl ester 43 ..... f J...... ■ ■ ■ i ‘ ■ 1 i ■ ■ ' ■ i ' ■ । । i 1 1 1 1 i 5.80 6.00 6.20 6.40 5000 127 m/z 125.00 8.69% 29 55 81 99
/z-> ................ ■q""। II ।1 ■' > i1 ltLll, —TP 109 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I’ INIISII 152 170
Abundance #4108: Hexanoic acid, 9-decen-1-yl ester J.... . ' ' I ■ ■ ■ ' i ■ ‘ 43 5.80 6.00 6.20 6.40 m/z 96.90 6.43% 29 5000 55 117 71 99 83 ....In.. A I » | l . . l-J-T 1’ I TI I I 1 11 1"! ITT | m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 5.80 6.00 6.20 6.40
11154.D SCAN020507.M Thu May 16 14:37:46 2002 Page 3
NYC-WTC_000025560
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000024883
Laboratory report documenting GCMS analysis of sample AE10246 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024780
Laboratory report documenting GCMS analysis of sample AE10241 conducted on May 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024804
Laboratory report documenting GCMS analysis of sample AE10242 conducted on May 28, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024665
Laboratory report documenting GCMS analysis of sample AE11158 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024824
Laboratory report documenting GCMS analysis of sample AE10243 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024692
Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022561
Laboratory commentary noting no unusual compounds detected in the GCMS scan of sample AE11480 on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024366
Chain of custody record for GCMS analysis of sample AE10236 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045778
Gas chromatography-mass spectrometry report for sample AE10703 showing detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043792
Analytical report for sample AE09768 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000025494
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000025495
Laboratory log sheet recording Method 608 extraction parameters and sample counts for sample AE11423 in May 2002.
Filed in the same folder
NYC-WTC_000025499
Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
Filed in the same folder
NYC-WTC_000025508
Laboratory report of GCMS calibration data showing response values and detection limits for 15 volatile organic compounds on May 17-21, 2002.
Filed in the same folder
NYC-WTC_000025512
Laboratory report of GCMS reference standard analysis showing response values for 15 volatile organic compounds on May 17-21, 2002.
Filed in the same folder