GCMS blank analysis results for sample AE06303, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020408\0318LB.D Vial: 8 Acq On 8 Apr 2002 5:24 pm Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.69 0.15 ug/1 308457 Naphthalene-d8 15.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 28 4 Phenethylamine, N-methyl- .beta.,... 399 C18H37NO3Si3 010538-85-9 28 Abundance Scan 1976 (14.689 min): 0318LB.D (-1968) (-) m/ z 73.10 100.00% 73

5000 267 355 ............... 1 1 i ■ ' 1 1 I ' ■ ■ ■ 1 1 1 1 1 1 1 1 14.40 14.60 14.80 15.00 o1 I m/ z 267.00 40.37% m/z-> 50 100 150 200 250 300 350 400 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000 267 14.40 14.60 14.80 15.00 355 m/z 355.00 38.44% 45 0- ,' ' Li TI 96 133 165 123,223 247 4 2293 323 n/z-> 50 100 150 200 250 300 350 400 Abundance #115315: Cyclopentasiloxane, decamethyl- 73 1 1 1 1 ■ ' 1 i ’ 1 1 i ' ' ' ■ i ' ' 355 14.40 14.60 14.80 15.00 267 5000 m/z 356.10 11.45% s 45 0 I_ T I ............... 207 , __ _ 323 ।" । V । 1 I 1 ' ' 1 I 1 1 ' ' I ' ' 1 1 1 1 ’ ' 1 1 1 miz-> 50 100 150 200 250 300 350 400 Abundance #27959: Noradrenaline tetraTMS 73 14.40 14.60 14.80 15.00 m/z 268.00 11.34%

5000 102 355

45 147 442 0 111 1 TI m/z-> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00

0318LB.D SCANAPR0902.M Tue Apr 09 15:08:06 2002 Page 4

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