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GCMS analysis report, sample AE02336, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010558–000010576

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

; Data File C:\MSDCHEM\l\DATA\030402\2336.D Vial: 8 Acq On 4 Mar 2002 4:00 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.07 1.08 ug/L 492815 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRI... 573 C24H51NO5Si5 000000-00-0 47 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 43 Abundance Scan 992 (12.074 mln): 2336.D (-) m/z 73.10 100.00% 73

5000 267 355 11.80 12.0012.2012.40 119 154 193223 , 0- —**f —323mnmmmmnt m/z 267.00 33.96% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 TIPP mmpr 11.80 12.0012.2012.40 m/z 355.10 23.45%

0- . ........207.41. 323 r m/z-> 50 100 iso' 200 250'' 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 733

■ • i ■ ■111 1'11" 11111 11.80 12.00 12.20 12.40 5000 m/z74.10 9.20% 267 355

0-2.1 103133163193223.4.1, 323 .............. ....... n/z—> 50 100 150 200 250 300 '356' 400 450' 500 '550 Abundance#379385: 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRIMETHYLSILYLAMINO- 73 T T T 11.80 12.00 12.20 12.40 T

m/z 356.00 7.90%

5000i 355

0—48,123,147178,218251 207325, 396 440470 530560 Si , , J ! . I I | I IT,|I>..|.I ■ • i' ■'111 n..... m/z—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

2336.D 5080302.M Mon Mar 18 08:31:43 2002 Page 3

NYC-WTC_000010565

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NYC-WTC_000010565Source: NYC Law Department, mirrored locally

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