DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\0130B.D Vial: 1 Acq On : 26 Feb 2002 10:17 am Operator: Sample : lab blank 1/30 Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 Cyclopentasiloxane, decamet... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.06 ug/L 45977 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 78 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 3 N-(Trifluoroacetyl)-N,O,O',0''-t.. . 553 C22H42F3NO4S14 000000-00-0 38 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 37 Abundance Scan 812 (12.540 min): 0130B.D (-) m/z 73.00 100.00% 73

5000 267 355 -

45 12.20 12.40 12.60 12.80 0-— m/ z 266.90 45.78% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 12.20 12.40 12.60 12.80 m/z 355.00 42.44% 0- 1 ■ i ' 1 1 1 । ■ 1 1 1 । 1 1 ■ 207 ।’ 4I1 323 11 I miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

12.20 12.40 12.60 12.80 5000 267 m/ z 356.00 12.79% 355 45 0- 1 IIII' 1 .... 193.223 11 . 323 1111′1 I 1‘‘11+1}t‘‘I‘’ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #377151: N-(TrifluoroacetyI)-N,O,O',O"-tetrakis(trimethyl... 1 ■ i 1 1 ' ■ i ■ ■ 73 12.20 12.40 12.60 12.80 m/ Z 74.10 9.73% 355 5000

45 h 147 193 267 [ 538 0 ■ ■ । । ' 'i ' । । । ■ ■ ■ ■ । । । ■ ■ i ' 1 ■ 1 i 1 ' ■ 1 i ■ ' ■ ■ i ■ ' ‘ ■ i r ' ■ 1 I 1 ‘ ■ i 1 ’ i ■ ■ 1 ' i ' ' 1 ' I m/z—> 50 100 150 200 250 300 350 400 450 500 550 12.20 12.40 12.60 12.80

0130B.D HP022102.M Wed Feb 27 08:34:18 2002 Page 9

NYC-WTC_000004518