GCMS analysis results, sample AE06334, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020408\6334.D Vial: 18 Acq On 9 Apr 2002 2:41 am Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \ SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Formamide, N-methylthio Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.51 0.13 ug/1 88229 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-methylthio 75 C2H5NS 1000196-87-7 4 2 Acetohydroxamic Acid 75 C2H5NO2 000546-88-3/4 3 Acetohydroxamic Acid 75 C2H5NO2 000546-88-3 3 4 1,2,4-Butanetriol 106 C4H10O3 003068-00-6 2 Abundance Scan 74 (3.514 min): 6334. D (-70) (-) m/ z 75.10 100.00% 75

5000 87

■ ■ i ■ ■ ■ n 1 1 1 ' i

mz-> 0 mTT i""i" 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 49 m 84 m/z 3.20 3.40 87.10 3.60 3.80 41.37% Abundance #28517: Formamide, N-methylthio 75

5000 30 ■ ■ । ' । 3.20 3.40 3.60 3.80 4245 60 m/z 84.00 8.82% Ot +27.33,439141148, 55 ,| -72 i'11' I " " r IJ —mpmmpn m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3866: Acetohydroxamic Acid 43 —■!■.>>! 1 > i j x . i ! । . i ■ . ] 3.20 3.40 3.60 3.80 5000 m/z 49.05 7.38% 15 -30.2 40 , ,59 75

mz-> 12 i 18 0 TTp-rTTp-rt-- 2424433,444447...56.4. . . 72.... m 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #109999: Acetohydroxamic Acid —1, ........................ .... I X X I I . | 4(3 3.20 3.40 3.60 3.80 m/z 47.05 4.87% 5000 W Mwwkj). 75 0 4649 5356 60 65 69 | X I X X | X X X I | X X " | XX X X [ " i ■ " ‘ r '1 'T" " 11" 11" n I " " I " I . I I I I | . ' . 1 | X . . . | 1 X . X | . . l”|“ x 1 . | . . . T m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.40 3.60 3.80

6334.D SCANAPR0902 .M Tue Apr 09 15:20:20 2002 Page 5

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