DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB27\02387.D Vial: 3 ’ Acq On : 27 Feb 2002 4:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 8 2-METHYL-3,3-D2-AZIRIDINE Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 9.89 0.07 ug/L 31920 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 9 2 Formamide, N-methyl- (CAS) $$ N-... 59 C2H5NO 000123-39-7 4 3 Formamide, N-methyl- (CAS) $$ N-... 59 C2H5NO 000123-39-7 4 4 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 Abundance Scan 577 (9.887 min): 02387.D (-) m/z 59.10 100.00% 50

5000

0- TI’*—uuuOum—maum- 41 45 73 | 11000*1—0—0—— 84 M 9.60 m/ z 9.80 10.00 10.20 45.10 15.83%

1 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #500: 2-METHYL-3,3-D2-AZIRIDINE 20 58

5000 9.60 9.80 10.00 10.20 42 m/ z 44.00 13.72% 26 oh ss - 1111 ................ ......... TTT tI’ i ■ ■ ■ -1 ■ । ■ i ■ ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #632: Formamide, N-methyl- (CAS) $$ N-methylformamide $$ M... 50 30 9.60 5000 m/ z !58.10 12.46%

15 27 0- 5 .... I......... I' 10 15 20 25 ‘ ■ i" ■ ■ i ■ ■ ■ ■ i ■ ■ ■11" 1' i ■' I" " ।" " ।"1 ■ ।1 ■" ।" ‘ ■ i ■" ■ । “ 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #630: Formamide, N-methyl- (CAS) $$ N-methylformamide $$ M... 50 9.60 9.80 10.00 10.20 30 m/ z 43.10 11.10%

5000 A

15 19 2,7 41 44 I 0 " i " " 11 rii 11111111111 TTIWNI—uuTTT I'11 ■ i''11111 ■ ■ i1 ■'11'1 ■' i'1 " i1 ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 9.60 9.80 10.00 10.20

02387.D HP022102.M Thu Feb 28 08:47:16 2002 Page 10

NYC-WTC_000005059