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DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02

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Scanned page image, NYC-WTC_000004142
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\31505.D Vial: 6 Acq On : 1 Feb 2002 6:53 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 9 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

20.86 0.36 ug/L 248253 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA... 888 C24H72O12SH2 018919-94-3 64 2 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 35 3 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 35 4 Silane, [[4-[1,2 -bis[(trimethyls... 458 C20H42O4Si4 056114-62-6 35 Abundance Scan 1532 (20.864 min): 31505.D (-) m/ z 73.10 100.00% 73

355 5000 147 221 ............... ) ............ 281 401 0- — 45 117 191 327 . I , ... ' I 1 1 11 1 ' 1 20.60 20.80 21.00 21.20 m/z 355.10 54.81% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclododeca... 73 355

147 221 281 , .........,..................... 5000 20.60 20.80 21.00 21.20 m/z 147.10 38.69% 327. 401 191 ii ,i 1 111. 0— ■ i 1 miz-> 50 100 150 200 250 300 350) 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 t ............................. , 20.60 20.80 21.00 21.20 5000- 355 m/z 221.10 29.78%

147 267 295 , L 193 । “[mn III429 457 O—IT TIIT m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313243: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim... 1+1* A.......... I ' 1 73 20.60 20.80 21.00 21.20 m/z 281.10 24.80% A 5000 355 45

m/z-> 0 IT 50 100 133 150 193 223 200 250 281 300 350 "si 400 450 n..... 20.60 20.80 21.00 21.20

31505.D SCAN508.M Mon Feb 04 10:14:22 2002 Page 11

NYC-WTC_000004142

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NYC-WTC_000004142Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗

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