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GCMS reference standard results for sample AE00327, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.

NYC-WTC_000051165–000051178

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\0108R.D Vial: 2 Acq On : 10 Jan 2002 1:11 pm Operator: Sample : ref ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Diazene, diphenyl- (CAS) $$... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 23.40 0.10 ug/L 57267 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Diazene, diphenyl- (CAS) $$ Azob... 182 C12H10N2 000103-33-3 72 2 Azobenzene 182 C12H10N2 000103-33-3 72 3 1,2-DIPHENYLHYDRAZINE 182 C12H10N2 000000-00-0 72 4 Azobenzene 182 C12H10N2 000103-33-3 64 Abundance Scan 1754 (23.399 min): 0108R.D (-) m/z 77.10 100.00% 77

5000 51 ........ \......... 105 182 65 91 23.00 23.20 23.40 23.60 23.80 39 152 169 198 01TT i" " i' TPPTT |l...... —m .. ।. m/ z 51.00 29.32% n/z-> :20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 Abundance। #90087: Diazene, diphenyl- (CAS) $$ Azobenzene $$ Azobenzo... 77

5000 ■ i ■ ■

51 23.00 23.20 23.40 23.60 23.80 105 182 m/z 105.00 19.54% 27 39 63 152 0 11" r ......... '"'I"1' i" " i' ■1 ■ i • ■1 • i1' ■ 111 ■11 'I I'"'I ■ i" " i ■■ m/z-> 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 Abundance #90082: Azobenzene 77 i ' ' ■ ■ i ' ■ ' ■ i T-l-I-r-r 23.00 23.20 23.40 23.60 23.80 5000 m/z 182.00 18.87% 51 105 182 . 63 128 152 m/z-> 0 TIPWWIWWWIVWWTTHT 4 ............ '"I ■ i" '11" " i " " i' r " ' r " ■ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 "r"rri" Abundance #90112:1,2-DIPHENYLHYDRAZINE 77 23.00 23.20 23.40 23.60 23.80 m/z91.00 12.57%

5000 51 105 182

n/z-> 39 63 0 TPTTITTTTTTTTTT TTTTT 4 i ■ ■" i "1' i" " r " ■ i 152 111 "I — 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 X 23.00 23.20 23.40 23.60 23.80

0108R.D W042302.M Thu May 02 14:37:28 2002 Page 7

NYC-WTC_000051176

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NYC-WTC_000051176Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.989

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.988

machine-extracted · confidence unavailable · Check page ↗

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