GCMS analysis results for sample AE10304, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10304.D Vial: 7 Acq On 8 May 2002 6:41 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Diazene, dimethyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 7.74 0.32 ug/L 216204 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Diazene, dimethyl- 58 C2H6N2 000503-28-6 9/ 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0/9 3 1,3-Dioxane-2-propanol, 2-methyl- 160 C8H16O3 036651-31-7 7 4 Butanal, 2-methyl-_________________ 86 C5H10O 000096-17-3 5 Abundance Scan 793 (7.738 min): 10304.D (-785) (-) m/z 43.10 100.00%!

U 43

5000 58 WW—WMWy 87 98 I.... ......... 1 ' 1 1 ' ' ' I 1 1 ' ' I 1 1 ' ' I

„ll 1 1 i ■ ' 7.40 7.60 7.80 8.00 0- i ' ' 1 1 i 1 r m/ z 58.10 43.80% mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #6: Diazene, dimethyl- 15 \uu. 43 "Wrr 5000 1 1 i ■ 1 1 1 i 1 ’ 1 ■ । ■ 1 1 1 I ■ 1 1 1 i 28 58 7.40 7.60 7.80 8.00______ m/z 87.0.0 28.70% - 0— । TT - I । । । i i । i < it । >■ । । । । । । । । r f । i । । i i i । i i । । । i । i । । iiii । r T miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4163: 3-Pyrrolidinol 43 1| 1 1 1 i ' 1 1 ' i r ' ' ■ i 7.40 7.60 7.80 8.00 5000 m/ z 55.10 20.10% 87 57 68

m/z-> 0 < I I | I I । । | i—। I I | J I T' I |

10 20 30 40 ' —+77 m i । । 50 60 70 80 90 100 110 120 130 140 150 ' 1 1 1 1 1 1 I 1 1 1 1 I ' 1 1 11 1 ‘ ' 1 I r ' ' ' 1 1 '

Abundance #5776:1,3-Dioxane-2-propanol, 2-methyl- — 1 ' 1 1 1 ‘ ' 1 1 1 ' i ' 1 43 58 7.40 7.60 7.80 8.00 m/ z 59.20 18.71% 5000 84

0 ' ' ' | I . . ' | ! . ' , | . , . . | ■ 5944 ...69,... 191—— I ’ 1 1 ' I 145 TITTTT 1 r । ' 1 1 1 । ' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.40 7.60 7.80 8.00

10304.D 050102.M Thu May 09 13:50:24 2002 Page 11

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