GCMS analysis results for sample AE10304, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10304.D Vial: 7 Acq On 8 May 2002 6:41 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 Phenylethanolamine Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 10.38 0.32 ug/L 218478 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenylethanolamine 137 C8H11NO 007568-93-6 28 2 1,3,6-Octatriene, (Z,E)- 108 C8H12 022038-68-2 25 3 1,3-Cyclooctadiene, 5-bromo- 186 C8HllBr 090002-40-725 4 Bicyclo [2.2.1]hepta-2,5-dien-7-ol 108 C7H80 000822-80-0 23 Abundance Scan 1243 (10.382 min): 10304.D (-1238) (-) m/z 108.00 100.00% 79 108

A 5000 51 39 | ............ ..................... ' 1 1 1 1 1 1 | 11 1 i | i r । । | । । 91

m/z-> 01 20 l '1 r 1 111'1111'11 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i1 " ' i " '11" " ir " ' r 11' r 1 10.00 10.20 10.40 10.60 10.80 m/ z 79.10 99.12% Abundance #875: Phenylethanolamine 33

5000 1 I ' ' ' ' I ' 1 1 ' 1 1 1 ' ' 1 1 1 10.00 10.20 10.40 10.60 10.80 79 m/z 77.10 75.55% 107 0 39 51 I T^Tt Mh .... L ।1 ■ ■' ।'1111 ■ 91 .1. 118 137 ‘Y1 ■ " i1 "1 111.11.।. ITTITTT 11111111111111 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #30604:1,3,6-Octatriene, (Z,E)- 79 0 10.00 10.20 10.40 10.60 10.80 5000 93 m/z 107.00 68.92%

27 39 53 66 108 1 0 4 - 1TT# THT i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ - -1 > ■ - ■ । ■ ■ ■ ■ । ■ m/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #115951:1,3-Cyclooctadiene, 5-bromo- ........ 1............ ' I ' ' 1 ' I ' ’ ■ 1 I ' I ‘ ' I I I I ' I ■ I 70 107 10.00 10.20 10.40 10.60 10.80 m/z 51.00 34.83%

5000 91 39 27 5,1 65 — 122 132 142 158 186 m/z-> 0 + rh‘r — 111' ‘11" ■' i11" i1 1T]l 1111111' । ■> 11111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 10.00 10.20 10.40 10.60 10.80

10304.D 050102.M Thu May 09 13:50:24 2002 Page 12

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