GCMS analysis results for sample AE03075, March 5 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB28\02716 .D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 2-Propen-1-one, 1,3-diphenyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

33.64 0.04 ug/L 17248 Perylene-dl2 34.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2 - Propen-1-one, 1,3-diphenyl- 208 C15H120 000094-41-7 7 2 Chaicone $$ 2-Propen-1-one, 1,3-... 208 C15H120 000094-41-7 7 3 9-<1,1-(2)H(2)-ethyl)anthracene ... 208 C16H12D2 122875-86-9 7 4 Dibenzo[b,E]-1,4-diazabicyclo [2 .... 208 C14H12N2 094509-68-9 7 Abundance Scan 2681 (33.639 min): 02716.D (-) m/z 207.00 100.00% 207 49 191 281 WAAwML"WW 5000

33.40 33.60 33.80 34.00 oM • ■ i ■1 • ■ i • • ■ ‘ i ■ • ■ * । ■1 m/z 207.90 93.64% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 A Abundance #127959:2-Propen-1-one, 1,3-diphenyl- 207 A W 77 L 5000 131 ITE ’ I ‘ '

105 33.40 33.60 33.80 34.00 179 m/z 190.90 79.70%

0- mm 89 +r PBPIILOuT . 165 l , * > t ' ■ * • i 1 * * • i ' > * ' i * *- Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #127957: Chaicone $$ 2-Propen-1-one, 1,3-diphenyl- (CAS) $... 77 20/8

131 33.40 33.60 33.80 34.00 103 5000 m/z 280.90 73.75% 51

89 165 179 V AA Ui lit O—TT 1**** I ‘ ' I ' HP- * * ■ ■ i ‘ • i 1 ■ ■ • i • 1 ‘ ■ i ■ ' miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #125073: 9-(1,1-(2)H(2)-ethyI)anthracene $$ Anthracene, 9-... Tr 114**11* ‘ ‘ r 1 ‘ 191 208 33.40 33.60 33.80 34.00 m/z 49.00 71.58% Ml 5000 W 165 0■ i 1 1■1 i■1 ■ • i 1 ■ 1 ■i■ ■ ■ ■ i■ 1 ■ 1 i1 ■ ■ * I ■ ■ ■ 1 i■ ■ ■ ■ i' 1 ' l‘ • ! I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 33.40 33.60 33.80 34.00

02716.D HP022102.M Fri Mar 01 10:07:16 2002 Page 15

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