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GCMS analysis results for sample AE00276, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051040–000051054

Folder label: “GCMS X 1/7/02 A 1/8/02

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Scanned page image, NYC-WTC_000051052
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \MSDCHEM\1\5973N\02JAN08\276 .D Vial: 1 Acq On 8 Jan 2002 5:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.30 ug/L 189396 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 86 2 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 47 3 Anthracene-D10 188 C14D10 000000-00-0 45 4 7-methoxy-5-methylnaphthalen-2-ol 188 C12H1202 000000-00-0 45 Abundance Scan 1699 (22.771 min): 276.D (-) m/z 188.10 100.00% 188

5000

“■ i ' ■ ■ ■ i ' ' ■ r i 1 1 ' 1 I ' 1 1 ■ I 1 94 — 80 156 । 22.40 22.60 22.80 23.00 23.20 40 54 66 i 01 TTTTT ' | । ■ I ■ ' । . | . . . t ( ' I ! I | I । >11111111 ■ ■ ■ i'" ■ ....................... । । m/z 94.10 16.31% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

5000 22 40 22.60 22.80 23.00 23.20 m/z 189.10 14.01% 80 94 160 01 PPTTTTT 66 - TTTTr —1894 n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98584: 2,2,9,9-Tetramethyldec-5-ene-3,7-diyne 188 173 131 143 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.93% 77 158 119

n/z-> 01 11 | ri ' । rr''11" "i' " ■i' 40 50 60 70 80 IIUTTITTTTTT T’T ll11 TBTr "IITT 90 100 110 120 130 140 150 160 170 180 190 . — । । । । , , । । । , Abundance #84498: Anthracene-D10 188 22.40 22.60 22.80 23.00 23.20 m/ z 80.10 10.48%

5000 80 94 66 160 । 0 ------------- TTTur i ■ ■ ' ■ i ■ ' ' 1 I 1 n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

276.D SCAN508.M Wed Jan 09 15:16:16 2002 Page 9

NYC-WTC_000051052

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NYC-WTC_000051052Source: NYC Law Department, mirrored locally

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