Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
NYC-WTC_000050205–000050221Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report • Data File : C:\MSDCHEM\1\5973N\02JAN22\31647.D Vial: 3 Acq On : 22 Jan 2002 1:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Anthracene-dlO- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.36 ug/L 195176 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 000000-00-0 59 4 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H1202 055139-53-2 50 Abundance Scan 1699 (22.771 min): 31647.D (-) m/z 188.10 100.00% its
500)
94 66 80 2240 22.60 22.80 23.00 23.20 tntr TpTHr —Hr TBt m/z 94.05 16.51% miz-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188
5000 1 1 IPT 1 ‘ i ’ 1 ’ * i • 22.40 22.60 22.80 23.00 23.20 m/z 189.10 14.37% 80 94 160 66 m/z-> 1.1 ..I» 60 70 80 L 100 110 120 130 140 150 H 90 ................. 160 170 180 190 Abundance #84499: Phenanthrene-d10 188
22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 13.99%
80 94 160 66 niz-> 60 HPP 70 mHke 111111111 P 11111111111 > 11111
80 90 100 110 120 130 140 150 160 170 180 190 11...... W... Abundance #98580: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetra<ieca... 188 22.40 22.60 22.80 23.00 23.20 m/z 80.10 12.87%
5000 79 67 93 131 117__ L — — 11 ■ • • ■ i ■111 r‘1111'''11'111I 1''1111'11111 ‘I ’ * 159 IL ■ i ■ ■ ■ •(■••• i • n/z—> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20
31647.D SCAN508.M Thu Jan 24 13:55:41 2002 Page 11
NYC-WTC_000050219
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NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050240
Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051605
Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052108
Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050334
Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder