NYC-WTC_000051122
Laboratory report showing GCMS analysis of sample AE00319 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗Document / 14 pages
GCMS reference standard results for sample AE00327, Jan 2002
Machine-extracted title · confidence 100%Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
NYC-WTC_000051165–000051178Folder label: “GCMS X 1/8/02 A 1/10/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\0108R.D Vial: 2 Acq On : 10 Jan 2002 1:11 pm Operator: Sample : ref ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Piperidine, 1-(cyanoacetyl)... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
32.12 0.14 ug/L 83526 Chrysene-dl2 30.50 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Piperidine, 1-(cyanoacetyl)- $$ ... 152 C8H12N2O 015029-30-8 9 2 1-Methyl-l-(p-fluorophenyl)-l-si... 180 C10H13FSi 000000-00-0 9 3 1,4-Benzodioxan-2-ol $$ 1,4-Benz... 152 C8H803 005770-59-2 7 4 Benzoic acid, 3-methoxy-_____________ 152 C8H803 000586-38-9 7 Abundance Scan 2518 (32.122 min): 0108R. D (-) m/z 152.10 100.00% 152
5000
187 31.80 32.00 32.20 32.40 44 105 122 140 , 211 0 " i'1" i" " i" " r " ' r " ' i" " r " ■ r " ' i■ i " " (" " I ' ।. I'1'1 1 ' m/z 153.10 14.15% m/z-> i ■ ‘" i" " i 1 ‘ ■ ■ i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 1 Abundance #48849: Piperidine, 1-(cyanoacetyl)-$$ 1-Cyanoacetylpiper... 152
56 5000 42 68 84 31.80 32.00 32.20 32.40 112 97 m/z 151.00 5.30% 123 | | O+ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #86398:1 -Methyl-1 -(p-fluorophenyl)-l -silacyclobutane 152
31.80 32.00 32.20 32.40 5000 m/z 187.00 4.87% 137 90 123 180
m/z-> 0 105 TTTTTT LM 40 5Q 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 i' ‘ " I i" " i " " r "' i
Abundance #48742:1,4-Benzodioxan-2-ol $$ 1,4-Benzodioxin-2-ol, 2,3-... ■ ' I ' ' ' ■ I 152 31.80 32.00 32.20 32.40 m/z 105.20 3.60%
5000 109 ft 95 121 52 . 76
m/z-> 0 L64 Mispelurg ■An- 134
40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 r ' ■' r " ' r ■ ■' r " ' i "'' r "' i 31.80 32.00 32.20 32.40
0108R.D W042302.M Thu May 02 14:37:28 2002 Page 8
NYC-WTC_000051177
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NYC-WTC_000051177Source: NYC Law Department, mirrored locally
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NYC-WTC_000004935
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