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GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02

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Scanned page image, NYC-WTC_000004793
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\0201B.D Vial: I Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 1,2-Benzenedicarboxylic aci... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 20.00 0.12 ug/L 123473 Acenaphthene-dl0 18.34 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 222 C12H1404 000084-66-2 90 2 Diethyl Phthalate 222 C12H1404 000084-66-2 83 3 1,2-Benzenedicarboxylic acid, di... 222 C12H1404 000084-66-2 64 4 Diethyl Phthalate 222 C12H1404 000084-66-2 64 Abundance Scan 1456 (19.997 min): 0201 B.D (-) m/z 149.00 100.00% 149

5000

177 43 71 93 105' 121 19.60 19.80 20.00 20.20 20.40 O --++84. 1 TTT TITH j ■ > ■ i ■ ■ ■ • i > ■ • > ।11111 rn/z 177.10 20.32% nfe-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #147075:1,2-Benzenedicarboxylic acid, diethyl ester (CAS)... 149

5000 19.60 19.80 20.00 20.20 20.40 177 m/ Z 71.00 14.43% 50 /z—> 0 I"1....... 1'1" ■ 1 30 40 50 60 70 80 90 100110120130140150160170180190200210220 U 1l... 194..... 773. Abundance #147085: Diethyl Phthalate 149 A.......... 19.60 19.80 20.00 20.20 20.40 5000 m/z 176.00 11.94% 177 50 65 76 93 105 121

iz— > 0 mMHH+4+++++++132. U 30 40 50 60 70 80 90 100110120130140150160170180190200210220 222

Abundance #147077:1,2-Benzenedicarboxylic acid, diethyl ester (CAS)... 149 19.60 19.80 20.00 20.20 20.40 m/z 150.10 11.22% A 5000

177 50 65 76 93 105 121 132 m/z—> 0 -----TTT 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 .. ll......... 111773. 19.60 19.80 20.00 20.20 20.40

0201B.D SCAN508.M Thu Feb 21 10:18:58 2002 Page 10

NYC-WTC_000004793

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NYC-WTC_000004793Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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