DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02FEB27\02382.D Vial: 3 Acq On : 27 Feb 2002 12:13 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L

Peak Number 7 Diethyl Phthalate $$ 1,2-Be... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

20.00 0.08 ug/L 55439 Acenaphthene -dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Diethyl Phthalate $$ 1,2-Benzene... 222 C12H1404 000084-66-2 90 2 1,2-Benzenedicarboxylic acid, di... 222 C12H1404 000084-66-2 90 3 1,2-Benzenedicarboxylic acid, di... 222 C12H1404 000084-66-2 83 4 1,2-Benzenedicarboxylic acid, di... 222 C12H1404 000084-66-2 83 Abundance Scan 1473 (20.002 min): 02382.D (-) m/z 149.00 100.00% 149

5000

177 i ' 1 ■ ■ i ■ ■ i ■ ■ ■ ■ । ।

51 65 76 93 104 121 19.60 19.80 20.00 20.20 20.40 o1- ■ । ■ > । > । ■ ■ । ■ ।1' ■ ■ । ■ ■ ■ ■ । ■1 ■ ■ । ■ ■ ■ ■ 11 । > ■ ■ > । ■ TPTTT m/z 177.10 23.14% m/z-> 40 50 60 70 80 90 100110120130 140150 160170180 190 200 210 220 Abundance #147079: Diethyl Phthalate $$ 1,2-Benzenedicarboxylic acid... 149

5000 19.60 19.80 20.00 20.20 20.40 177 m/z 150.00 12.80%

/z-> 0- -ir 50 m 40 50 60 70 80 90 100110120130 140150160170180 190 200 11" " i । 210 220 222 " 11 ■ ■ ■ i

Abundance #147088:1,2-Benzenedicarboxylic acid, diethyl ester (CAS)... 149

19.60 19.80 20.00 20.20 20.40 5000 m/z 76.00 12.29% 177 50 65 76 93 105 121 132 222 0 noongdsagoogkol. - - ■ ■ ] ■ ■ ■ ■ i ■ ■ ■ ■ i ■ - ■ ■ i1 ■ ‘ ■ i

miz-> 40 50 60 70 80 90 100110120130 140150160170 180 190 200 210 220 Abundance #147075:1,2-Benzenedicarboxylic acid, diethyl ester (CAS)... 149 19.60 19.80 20.00 20.20 20.40 m/z 65.00 12.07%

5000 177 50 65 76 93 105 121 132 , 222 0 i" " i" HT m/z-> 40 50 60 70 80 90 100110120130 140150160170180 190 200 210 220 19.60 19.80 20.00 20.20 20.40

32382.D HP022102.M Thu Feb 28 08:46:48 2002 Page 9

NYC-WTC_000004978

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999